- Development of an HPLC-UV-Vis Method for the Determination of Epirubicin Residues on Stainless-Steel Surfaces. [Journal Article]J AOAC Int. 2026 Oct 28. [Online ahead of print]JA
- CONCLUSIONS: The developed HPLC-UV-Vis method showed suitable chromatographic performance for epirubicin determination under the investigated solution-based conditions and was applied to residue monitoring in swab samples collected from stainless-steel surfaces following cleaning. Because surface recovery was assessed at only one spiking level, the complete surface-sampling and extraction procedure was not comprehensively validated.
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- Validation of a lateral flow assay for the qualitative detection of okadaic acid-group toxins in shellfish. [Journal Article]J AOAC Int. 2026 Oct 27. [Online ahead of print]JA
- CONCLUSIONS: The Sensoreal DSP Alert™ LFA is a robust, sensitive, and user-friendly screening method for qualitative determination of OA-group toxins in bivalve mollusk shellfish. The assay demonstrated excellent agreement with the LC-MS/MS reference method, no false-negative results at the selected decision threshold, reliable ruggedness, and strong selectivity. The scanner-based Low/Medium/High classification provides additional practical value for shellfish hazard management and end-product testing.
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- Development of a Simple and Rapid HPLC-UV Method for Simultaneous Determination of Ciprofloxacin Hydrochloride and Oxytetracycline Hydrochloride in Aqueous Matrix. [Journal Article]J AOAC Int. 2026 Oct 20. [Online ahead of print]JA
- CONCLUSIONS: The HPLC-UV approach was applicable for the simultaneous determination of CIP and OTC in aqueous samples containing relatively elevated concentrations of the target antibiotics. The method is not intended for direct trace-level determination in typical environmental waters without an appropriate preconcentration step.
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- Current Applications of Hyperspectral Imaging Techniques Combined with Chemometrics for Food Analysis. [Journal Article]J AOAC Int. 2026 Oct 15. [Online ahead of print]JA
- With the growing demand for high-quality and safe food products, innovations in food detection methods are becoming increasingly important. Hyperspectral imaging (HSI) technique combined with chemometrics, has emerged as an efficient, non-destructive, and high-precision approach, offering innovative solutions for food quality and safety analysis in the food sector. HSI technology enables the simu…
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- Non-Targeted LC-Q-Orbitrap HRMS Screening of Veterinary Drugs, Pesticides, and Emerging Contaminants in Animal-Derived Foods and Honey. [Journal Article]J AOAC Int. 2026 Oct 15. [Online ahead of print]JA
- CONCLUSIONS: HRMS-based non-targeted screening extends analytical coverage beyond predefined reference-standard panels in multi-matrix food surveillance.
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- Evaluation of Three Automated Pretreatment Workstations for Free Silica Determination. [Journal Article]J AOAC Int. 2026 Oct 10. [Online ahead of print]JA
- CONCLUSIONS: All three workstations are safe, reliable alternatives to manual PPA digestion and agreed with the manual method on field samples.
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- Research progress on identification and quality control analysis of Eupolyphaga sinensis Walker. [Journal Article]J AOAC Int. 2026 Oct 08. [Online ahead of print]JA
- Eupolyphaga sinensis Walker is an important animal-derived medicinal material, yet the analytical evidence supporting its authentication and quality control has not been critically mapped across method classes. This scoping review, reported with reference to the PRISMA Extension for Scoping Reviews (PRISMA-ScR), maps methods used for Eupolyphaga sinensis Walker, related or confounding materials, …
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- Research Progress on Proteomics-Based Detection Techniques for Meat Adulteration. [Journal Article]J AOAC Int. 2026 Oct 01. [Online ahead of print]JA
- CONCLUSIONS: Proteomics provides high-resolution, multi-target analytical capabilities for complex matrices. Future directions for this field include the translation of technological into biosensors and the global standardization of peptide libraries. Potential leadership for these efforts could come from international organizations, with the aim of advancing industrial and regulatory applications.
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- Rapid Detection of Component Contents in Polyphenol-Rich Plant Leaves Based on Near-Infrared Spectroscopy. [Journal Article]J AOAC Int. 2026 Sep 30. [Online ahead of print]JA
- CONCLUSIONS: The results demonstrate that near-infrared spectroscopy combined with chemometric methods demonstrates high predictive capability and practical application value for the quantitative determination of tannic acid, gallic acid, and moisture in polyphenol-rich plant leaves.
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- Determination of cadmium, lead and mercury in cannabis flowers by microwave plasma atomic emission spectrometry. [Journal Article]J AOAC Int. 2026 Sep 24. [Online ahead of print]JA
- CONCLUSIONS: MP AES and CV-MP AES provide adequate accuracy and precision for the determination of Cd, Pb, and Hg in cannabis flowers. The proposed methodologies represent a practical, cost-effective, and sustainable alternative to argon-based plasma techniques for routine quality control and compliance testing of cannabis products.
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- A Risk-Based Framework to Optimize Microbiological Testing of Primary Packaging Materials. [Journal Article]J AOAC Int. 2026 Sep 24. [Online ahead of print]JA
- CONCLUSIONS: These findings support a risk-based strategy to optimize the frequency of microbiological testing. Historical microbiological performance represents the primary basis for reduced testing, while Aw and material attributes provide complementary evidence. This approach enables optimization of testing under controlled conditions without replacing microbiological control, in alignment with ICH Q9(R1), ICH Q6A, and relevant compendial guidance.
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- Edible Fish as a Source of Klebsiella pneumoniae: Incidence, Virulence, Biofilm Formation, Antimicrobial Resistance and Control Strategies. [Journal Article]J AOAC Int. 2026 Sep 21. [Online ahead of print]JA
- CONCLUSIONS: The present study showed majority of the K. pneumoniae isolates from seafood were found to be virulent, multidrug-resistant, ESBL producers, and moderate biofilm formers indicating potential health risk to fish consumers. Water-soluble chitosan showed a significant inhibitory effect on growth of all K. pneumoniae isolates.
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- Evaluating Substitution of Hazardous Solvents in USP Monograph HPLC Methods. [Journal Article]J AOAC Int. 2026 Sep 10. [Online ahead of print]JA
- CONCLUSIONS: Greener solvents are highly likely to replace hazardous solvents used in compendial chromatography methods without loss of performance.
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- STRATUM-Structured Framework for Reporting, Assessment, and Translational Utility of Metagenomics. [Journal Article]J AOAC Int. 2026 Sep 09. [Online ahead of print]JA
- CONCLUSIONS: Realizing the operational potential of mNGS requires evidentiary standards responsive to decision context rather than fixed across applications. STRATUM offers a consequence-tiered model for quality and reporting in applied metagenomics, supporting reproducible, transparent, and defensible sequencing-based surveillance across public health and biodefense domains.
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