Sturzbecher-Höhne M, Kissner R, Nauser T, Koppenol WH
Preparation and properties of lithium and sodium peroxynitrite. [Journal Article, Research Support, Non-U.S. Gov't]
Chem Res Toxicol 2008 Dec; 21(12):2257-9.
We describe the preparation of aqueous solutions of LiONOO and NaONOO from (Me4N)ONOO. An aqueous solution of analytically pure, commercially available (Me4N)ONOO is applied to an Amberlyst 15 column at 4 degrees C, and the Me4N+ is rapidly (in 20 min) exchanged against Li+ or Na+. The exchanged peroxynitrite is produced in yields of ca. 90% with a nitrite content of 5-6%.
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