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[Simultaneous analysis and detection of pesticides in fresh fruits and vegetables by HPLC and GC].

Abstract

A method was established for simultaneous determination of pesticide residue in fresh fruits and vegetables by HPLC and GC. CH3CN extraction/NaCl partiton method was used in order to recover hydrophilic pesticide such as acephate, methamidophos. Dimethoate and methamidophos from okra and DDVP from strawberry were detected by GC. On the other hand confirmation method by GC and GC/MS was studied for peaks detected by HPLC with UV and/or FL detector. OPP, TBZ, imazalil chlorpyrifos etc. in citrus fruits were detected by the proposed method.

Authors

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Pub Type(s)

English Abstract
Journal Article

Language

jpn

PubMed ID

10097528

Citation

Tsuchiya, T, et al. "[Simultaneous Analysis and Detection of Pesticides in Fresh Fruits and Vegetables By HPLC and GC]." Kokuritsu Iyakuhin Shokuhin Eisei Kenkyujo Hokoku = Bulletin of National Institute of Health Sciences, 1998, pp. 157-62.
Tsuchiya T, Maeda K, Sekiguchi Y, et al. [Simultaneous analysis and detection of pesticides in fresh fruits and vegetables by HPLC and GC]. Kokuritsu Iyakuhin Shokuhin Eisei Kenkyusho Hokoku. 1998.
Tsuchiya, T., Maeda, K., Sekiguchi, Y., Hirahara, Y., Watanabe, Y., & Tonogai, Y. (1998). [Simultaneous analysis and detection of pesticides in fresh fruits and vegetables by HPLC and GC]. Kokuritsu Iyakuhin Shokuhin Eisei Kenkyujo Hokoku = Bulletin of National Institute of Health Sciences, (116), 157-62.
Tsuchiya T, et al. [Simultaneous Analysis and Detection of Pesticides in Fresh Fruits and Vegetables By HPLC and GC]. Kokuritsu Iyakuhin Shokuhin Eisei Kenkyusho Hokoku. 1998;(116)157-62. PubMed PMID: 10097528.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Simultaneous analysis and detection of pesticides in fresh fruits and vegetables by HPLC and GC]. AU - Tsuchiya,T, AU - Maeda,K, AU - Sekiguchi,Y, AU - Hirahara,Y, AU - Watanabe,Y, AU - Tonogai,Y, PY - 1999/3/31/pubmed PY - 1999/3/31/medline PY - 1999/3/31/entrez SP - 157 EP - 62 JF - Kokuritsu Iyakuhin Shokuhin Eisei Kenkyujo hokoku = Bulletin of National Institute of Health Sciences JO - Kokuritsu Iyakuhin Shokuhin Eisei Kenkyusho Hokoku IS - 116 N2 - A method was established for simultaneous determination of pesticide residue in fresh fruits and vegetables by HPLC and GC. CH3CN extraction/NaCl partiton method was used in order to recover hydrophilic pesticide such as acephate, methamidophos. Dimethoate and methamidophos from okra and DDVP from strawberry were detected by GC. On the other hand confirmation method by GC and GC/MS was studied for peaks detected by HPLC with UV and/or FL detector. OPP, TBZ, imazalil chlorpyrifos etc. in citrus fruits were detected by the proposed method. SN - 1343-4292 UR - https://www.unboundmedicine.com/medline/citation/10097528/[Simultaneous_analysis_and_detection_of_pesticides_in_fresh_fruits_and_vegetables_by_HPLC_and_GC]_ DB - PRIME DP - Unbound Medicine ER -