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Simultaneous screening and detection of drugs in small blood samples and bloodstains.
Forensic Sci Int. 2002 May 23; 126(3):191-6.FS

Abstract

A gas chromatography-mass spectrometry (GC-MS) method is described for the screening and detection of morphine, codeine, cocaine, benzoylecgonine, methylecgonine, cocaethylene, delta-9-tetrahydrocannabinol (THC), 11-nor-9-carboxy-THC (THC-COOH), 11-hydroxy-THC (11-OH-THC), amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymetamphetamine (MDMA) and N-methyl-1-(3,4-methylenedioxyphenyl)-2-butanamine (MBDB) in small blood samples and bloodstains using solid phase SPE columns and a pipetting robot (Gilson Aspec XL). The detection limits are in the order of 1.62-4.10 ng/50 microl spot (amphetamines), 0.15-0.82 ng/50 microl spot (cannabinoids), 1.67-4.70 ng/50 microl spot (cocaine and derivatives) and 4.53-4.91 ng/50 microl spot (opiates) and the correlation factors are between 0.9957 and 0.9999. The method has proven useful in forensic cases with only small sample volumes or bloodstains.

Authors+Show Affiliations

Institute of Legal Medicine, University Giessen, Frankfurter Str 58, D-35392 Giessen, Germany. harald.f.schuetz@forens-med.uni-giessen.deNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Case Reports
Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

12062939

Citation

Schütz, Harald, et al. "Simultaneous Screening and Detection of Drugs in Small Blood Samples and Bloodstains." Forensic Science International, vol. 126, no. 3, 2002, pp. 191-6.
Schütz H, Gotta JC, Erdmann F, et al. Simultaneous screening and detection of drugs in small blood samples and bloodstains. Forensic Sci Int. 2002;126(3):191-6.
Schütz, H., Gotta, J. C., Erdmann, F., Risse, M., & Weiler, G. (2002). Simultaneous screening and detection of drugs in small blood samples and bloodstains. Forensic Science International, 126(3), 191-6.
Schütz H, et al. Simultaneous Screening and Detection of Drugs in Small Blood Samples and Bloodstains. Forensic Sci Int. 2002 May 23;126(3):191-6. PubMed PMID: 12062939.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Simultaneous screening and detection of drugs in small blood samples and bloodstains. AU - Schütz,Harald, AU - Gotta,Jan Christoph, AU - Erdmann,Freidoon, AU - Risse,Manfred, AU - Weiler,Günter, PY - 2002/6/14/pubmed PY - 2002/11/26/medline PY - 2002/6/14/entrez SP - 191 EP - 6 JF - Forensic science international JO - Forensic Sci Int VL - 126 IS - 3 N2 - A gas chromatography-mass spectrometry (GC-MS) method is described for the screening and detection of morphine, codeine, cocaine, benzoylecgonine, methylecgonine, cocaethylene, delta-9-tetrahydrocannabinol (THC), 11-nor-9-carboxy-THC (THC-COOH), 11-hydroxy-THC (11-OH-THC), amphetamine, methamphetamine, 3,4-methylenedioxyamphetamine (MDA), 3,4-methylenedioxymetamphetamine (MDMA) and N-methyl-1-(3,4-methylenedioxyphenyl)-2-butanamine (MBDB) in small blood samples and bloodstains using solid phase SPE columns and a pipetting robot (Gilson Aspec XL). The detection limits are in the order of 1.62-4.10 ng/50 microl spot (amphetamines), 0.15-0.82 ng/50 microl spot (cannabinoids), 1.67-4.70 ng/50 microl spot (cocaine and derivatives) and 4.53-4.91 ng/50 microl spot (opiates) and the correlation factors are between 0.9957 and 0.9999. The method has proven useful in forensic cases with only small sample volumes or bloodstains. SN - 0379-0738 UR - https://www.unboundmedicine.com/medline/citation/12062939/Simultaneous_screening_and_detection_of_drugs_in_small_blood_samples_and_bloodstains_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0379073802000531 DB - PRIME DP - Unbound Medicine ER -