Tags

Type your tag names separated by a space and hit enter

Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry.
Anal Chem. 2002 Jul 01; 74(13):3071-5.AC

Abstract

Amphetamine, methamphetamine, and their methylenedioxy derivatives have been identified and measured in a human urine matrix using solid-phase microextraction (SPME) and high-field asymmetric waveform ion mobility spectrometry (FAIMS) in combination with electrospray ionization (ESI) and mass spectrometric detection (MS). Limits of detection in human urine between 200 pg/mL and 7.5 ng/mL have been achieved. The use of a simple extraction method, SPME, combined with the high sensitivity and selectivity of ESI-FAIMS-MS eliminates the need for chromatographic separation and allows for very rapid sample processing.

Authors+Show Affiliations

Institute for National Measurement Standards, National Research Council of Canada, Ottawa, ON.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

12141666

Citation

McCooeye, Margaret A., et al. "Quantitation of Amphetamine, Methamphetamine, and Their Methylenedioxy Derivatives in Urine By Solid-phase Microextraction Coupled With Electrospray Ionization-high-field Asymmetric Waveform Ion Mobility Spectrometry-mass Spectrometry." Analytical Chemistry, vol. 74, no. 13, 2002, pp. 3071-5.
McCooeye MA, Mester Z, Ells B, et al. Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry. Anal Chem. 2002;74(13):3071-5.
McCooeye, M. A., Mester, Z., Ells, B., Barnett, D. A., Purves, R. W., & Guevremont, R. (2002). Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry. Analytical Chemistry, 74(13), 3071-5.
McCooeye MA, et al. Quantitation of Amphetamine, Methamphetamine, and Their Methylenedioxy Derivatives in Urine By Solid-phase Microextraction Coupled With Electrospray Ionization-high-field Asymmetric Waveform Ion Mobility Spectrometry-mass Spectrometry. Anal Chem. 2002 Jul 1;74(13):3071-5. PubMed PMID: 12141666.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry. AU - McCooeye,Margaret A, AU - Mester,Zoltán, AU - Ells,Barbara, AU - Barnett,David A, AU - Purves,Randy W, AU - Guevremont,Roger, PY - 2002/7/27/pubmed PY - 2002/9/7/medline PY - 2002/7/27/entrez SP - 3071 EP - 5 JF - Analytical chemistry JO - Anal Chem VL - 74 IS - 13 N2 - Amphetamine, methamphetamine, and their methylenedioxy derivatives have been identified and measured in a human urine matrix using solid-phase microextraction (SPME) and high-field asymmetric waveform ion mobility spectrometry (FAIMS) in combination with electrospray ionization (ESI) and mass spectrometric detection (MS). Limits of detection in human urine between 200 pg/mL and 7.5 ng/mL have been achieved. The use of a simple extraction method, SPME, combined with the high sensitivity and selectivity of ESI-FAIMS-MS eliminates the need for chromatographic separation and allows for very rapid sample processing. SN - 0003-2700 UR - https://www.unboundmedicine.com/medline/citation/12141666/Quantitation_of_amphetamine_methamphetamine_and_their_methylenedioxy_derivatives_in_urine_by_solid_phase_microextraction_coupled_with_electrospray_ionization_high_field_asymmetric_waveform_ion_mobility_spectrometry_mass_spectrometry_ L2 - https://doi.org/10.1021/ac011296+ DB - PRIME DP - Unbound Medicine ER -