Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry.Anal Chem. 2002 Jul 01; 74(13):3071-5.AC
Abstract
Amphetamine, methamphetamine, and their methylenedioxy derivatives have been identified and measured in a human urine matrix using solid-phase microextraction (SPME) and high-field asymmetric waveform ion mobility spectrometry (FAIMS) in combination with electrospray ionization (ESI) and mass spectrometric detection (MS). Limits of detection in human urine between 200 pg/mL and 7.5 ng/mL have been achieved. The use of a simple extraction method, SPME, combined with the high sensitivity and selectivity of ESI-FAIMS-MS eliminates the need for chromatographic separation and allows for very rapid sample processing.
MeSH
Pub Type(s)
Journal Article
Language
eng
PubMed ID
12141666
Citation
McCooeye, Margaret A., et al. "Quantitation of Amphetamine, Methamphetamine, and Their Methylenedioxy Derivatives in Urine By Solid-phase Microextraction Coupled With Electrospray Ionization-high-field Asymmetric Waveform Ion Mobility Spectrometry-mass Spectrometry." Analytical Chemistry, vol. 74, no. 13, 2002, pp. 3071-5.
McCooeye MA, Mester Z, Ells B, et al. Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry. Anal Chem. 2002;74(13):3071-5.
McCooeye, M. A., Mester, Z., Ells, B., Barnett, D. A., Purves, R. W., & Guevremont, R. (2002). Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry. Analytical Chemistry, 74(13), 3071-5.
McCooeye MA, et al. Quantitation of Amphetamine, Methamphetamine, and Their Methylenedioxy Derivatives in Urine By Solid-phase Microextraction Coupled With Electrospray Ionization-high-field Asymmetric Waveform Ion Mobility Spectrometry-mass Spectrometry. Anal Chem. 2002 Jul 1;74(13):3071-5. PubMed PMID: 12141666.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR
T1 - Quantitation of amphetamine, methamphetamine, and their methylenedioxy derivatives in urine by solid-phase microextraction coupled with electrospray ionization-high-field asymmetric waveform ion mobility spectrometry-mass spectrometry.
AU - McCooeye,Margaret A,
AU - Mester,Zoltán,
AU - Ells,Barbara,
AU - Barnett,David A,
AU - Purves,Randy W,
AU - Guevremont,Roger,
PY - 2002/7/27/pubmed
PY - 2002/9/7/medline
PY - 2002/7/27/entrez
SP - 3071
EP - 5
JF - Analytical chemistry
JO - Anal Chem
VL - 74
IS - 13
N2 - Amphetamine, methamphetamine, and their methylenedioxy derivatives have been identified and measured in a human urine matrix using solid-phase microextraction (SPME) and high-field asymmetric waveform ion mobility spectrometry (FAIMS) in combination with electrospray ionization (ESI) and mass spectrometric detection (MS). Limits of detection in human urine between 200 pg/mL and 7.5 ng/mL have been achieved. The use of a simple extraction method, SPME, combined with the high sensitivity and selectivity of ESI-FAIMS-MS eliminates the need for chromatographic separation and allows for very rapid sample processing.
SN - 0003-2700
UR - https://www.unboundmedicine.com/medline/citation/12141666/Quantitation_of_amphetamine_methamphetamine_and_their_methylenedioxy_derivatives_in_urine_by_solid_phase_microextraction_coupled_with_electrospray_ionization_high_field_asymmetric_waveform_ion_mobility_spectrometry_mass_spectrometry_
DB - PRIME
DP - Unbound Medicine
ER -
