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[SFE-CGC determination of tanshinone in Salvia miltiorrhiza Bunge].
Yao Xue Xue Bao. 2001 Jan; 36(1):55-7.YX

Abstract

AIM

To analyze tanshinone IIA in Salvia miltiorrhiza Bunge by supercritical fluid extraction (SFE) coupled with capillary gas chromatography (CGC).

METHODS

The solution pressure was predicted by solubility parameter theory, the extraction conditions were confirmed by orthogonal design in which temperature, volume of modifier and dynamic extracting volume had been studied in three levels.

RESULTS

This method is quick, convenient, precise and accurate, added sample recovery is 95.3%, RSD = 4.27%.

CONCLUSION

Compared with the method of ultrasonic extraction, significantly better qualitative and quantitative result could be obtained by SFE-CGC and expend less organic solvent then make less pollution.

Authors+Show Affiliations

Chen B
School of Pharmacy, Second Military Medical University, Shanghai 200433, China. chenbin-sh@hotmail.com
Zhu M
No affiliation info available
Xing WX
No affiliation info available
Liu LL
No affiliation info available
Wu YT
No affiliation info available

MeSH

AbietanesChromatography, GasChromatography, Supercritical FluidPhenanthrenesPlants, MedicinalSalvia miltiorrhiza

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

12579862

Citation

Chen, B, et al. "[SFE-CGC Determination of Tanshinone in Salvia Miltiorrhiza Bunge]." Yao Xue Xue Bao = Acta Pharmaceutica Sinica, vol. 36, no. 1, 2001, pp. 55-7.
Chen B, Zhu M, Xing WX, et al. [SFE-CGC determination of tanshinone in Salvia miltiorrhiza Bunge]. Yao Xue Xue Bao. 2001;36(1):55-7.
Chen, B., Zhu, M., Xing, W. X., Liu, L. L., & Wu, Y. T. (2001). [SFE-CGC determination of tanshinone in Salvia miltiorrhiza Bunge]. Yao Xue Xue Bao = Acta Pharmaceutica Sinica, 36(1), 55-7.
Chen B, et al. [SFE-CGC Determination of Tanshinone in Salvia Miltiorrhiza Bunge]. Yao Xue Xue Bao. 2001;36(1):55-7. PubMed PMID: 12579862.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [SFE-CGC determination of tanshinone in Salvia miltiorrhiza Bunge]. AU - Chen,B, AU - Zhu,M, AU - Xing,W X, AU - Liu,L L, AU - Wu,Y T, PY - 2003/2/13/pubmed PY - 2003/8/9/medline PY - 2003/2/13/entrez SP - 55 EP - 7 JF - Yao xue xue bao = Acta pharmaceutica Sinica JO - Yao Xue Xue Bao VL - 36 IS - 1 N2 - AIM: To analyze tanshinone IIA in Salvia miltiorrhiza Bunge by supercritical fluid extraction (SFE) coupled with capillary gas chromatography (CGC). METHODS: The solution pressure was predicted by solubility parameter theory, the extraction conditions were confirmed by orthogonal design in which temperature, volume of modifier and dynamic extracting volume had been studied in three levels. RESULTS: This method is quick, convenient, precise and accurate, added sample recovery is 95.3%, RSD = 4.27%. CONCLUSION: Compared with the method of ultrasonic extraction, significantly better qualitative and quantitative result could be obtained by SFE-CGC and expend less organic solvent then make less pollution. SN - 0513-4870 UR - https://www.unboundmedicine.com/medline/citation/12579862/[SFE_CGC_determination_of_tanshinone_in_Salvia_miltiorrhiza_Bunge]_ DB - PRIME DP - Unbound Medicine ER -