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[Selective isolation of anethole from volatile oil of Foeniculum vulgare Mill by inclusion crystalline with chela-shape host].
Yao Xue Xue Bao. 2001 Sep; 36(9):672-5.YX

Abstract

AIM

To isolate the components from the volatile oil of Foeniculum vulgare Mill.

METHODS

According to the function of molecular recognition of supramolecular chemistry, chela shape molecule, trans-1, 2-biphenyl-1, 2-acenaphthendiol was used as host molecule and the volatile oil of Foeniculum vulgare Mill as guest molecule. Trans-1, 2-biphenyl-1, 2-acenaphthendiol can recognize the components that endowed with interactional complementarity and form inclusion compound as crystals.

RESULTS

The anethole in the volatile oil was selectively included as trans-1,2-biphenyl-1,2-acenaphthendiol which was obtained in pure state from the inclusion compound by Kugelrohr vacuum technology. The formation of inclusion compound was confirmed by means of IR and powder XRD. The structure of the selectively isolated component was elucidated as trans-anethole by means of IR, 1HMMR and MS.

CONCLUSION

The experimental results showed that the method is simple, rapid and selective for isolation anethole from volatile oil of Foeniculum vulgare Mill.

Authors+Show Affiliations

Institute of Chemical Science and Engineering, Liaoning University, Shenyang 110036, China.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

12580105

Citation

Xia, Z H., et al. "[Selective Isolation of Anethole From Volatile Oil of Foeniculum Vulgare Mill By Inclusion Crystalline With Chela-shape Host]." Yao Xue Xue Bao = Acta Pharmaceutica Sinica, vol. 36, no. 9, 2001, pp. 672-5.
Xia ZH, Guo WS, Tang XD, et al. [Selective isolation of anethole from volatile oil of Foeniculum vulgare Mill by inclusion crystalline with chela-shape host]. Yao Xue Xue Bao. 2001;36(9):672-5.
Xia, Z. H., Guo, W. S., Tang, X. D., Wang, X. M., Tong, J., You, J., Cai, Y. P., & Lu, Y. (2001). [Selective isolation of anethole from volatile oil of Foeniculum vulgare Mill by inclusion crystalline with chela-shape host]. Yao Xue Xue Bao = Acta Pharmaceutica Sinica, 36(9), 672-5.
Xia ZH, et al. [Selective Isolation of Anethole From Volatile Oil of Foeniculum Vulgare Mill By Inclusion Crystalline With Chela-shape Host]. Yao Xue Xue Bao. 2001;36(9):672-5. PubMed PMID: 12580105.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Selective isolation of anethole from volatile oil of Foeniculum vulgare Mill by inclusion crystalline with chela-shape host]. AU - Xia,Z H, AU - Guo,W S, AU - Tang,X D, AU - Wang,X M, AU - Tong,J, AU - You,J, AU - Cai,Y P, AU - Lu,Y, PY - 2003/2/13/pubmed PY - 2004/2/10/medline PY - 2003/2/13/entrez SP - 672 EP - 5 JF - Yao xue xue bao = Acta pharmaceutica Sinica JO - Yao Xue Xue Bao VL - 36 IS - 9 N2 - AIM: To isolate the components from the volatile oil of Foeniculum vulgare Mill. METHODS: According to the function of molecular recognition of supramolecular chemistry, chela shape molecule, trans-1, 2-biphenyl-1, 2-acenaphthendiol was used as host molecule and the volatile oil of Foeniculum vulgare Mill as guest molecule. Trans-1, 2-biphenyl-1, 2-acenaphthendiol can recognize the components that endowed with interactional complementarity and form inclusion compound as crystals. RESULTS: The anethole in the volatile oil was selectively included as trans-1,2-biphenyl-1,2-acenaphthendiol which was obtained in pure state from the inclusion compound by Kugelrohr vacuum technology. The formation of inclusion compound was confirmed by means of IR and powder XRD. The structure of the selectively isolated component was elucidated as trans-anethole by means of IR, 1HMMR and MS. CONCLUSION: The experimental results showed that the method is simple, rapid and selective for isolation anethole from volatile oil of Foeniculum vulgare Mill. SN - 0513-4870 UR - https://www.unboundmedicine.com/medline/citation/12580105/[Selective_isolation_of_anethole_from_volatile_oil_of_Foeniculum_vulgare_Mill_by_inclusion_crystalline_with_chela_shape_host]_ DB - PRIME DP - Unbound Medicine ER -