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[Determination of cirsilineol in Herba Artemisiae scopariae collected in autumn by HPLC].
Zhongguo Zhong Yao Za Zhi. 2002 Jan; 27(1):23-5.ZZ

Abstract

OBJECTIVE

To establish a quantitative method for determination of cirsilineol in Herba Artemisiae Scopariae collected in Autumn.

METHOD

Sample was extracted with methanol, and cleaned up with polyamide column. ODS column was used with methanol-acetonitrile-0.5% acetic acid solution (24:19:57) as mobile phase. Detection wavelength was 347 nm.

RESULT

Cirsilineol in sample solution was well separated. Linearity of cirsilineol was good (r = 0.9998) in range of 0.1-0.8 microgram. The average recovery was 101.3%, RSD of repeatability was 3.04%.

CONCLUSION

This method can be used for quality control of Herba Artemisiae Scopariae collected in autumn and its preparations.

Authors+Show Affiliations

Zhang QW
Institute of Chinese Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China.
Zhang YX
No affiliation info available
Zhang Y
No affiliation info available
Liang GG
No affiliation info available

MeSH

ArtemisiaChromatography, High Pressure LiquidFlavonesFlavonoidsPlants, MedicinalQuality ControlSeasons

Pub Type(s)

English Abstract
Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

12774348

Citation

Zhang, Qi-wei, et al. "[Determination of Cirsilineol in Herba Artemisiae Scopariae Collected in Autumn By HPLC]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 27, no. 1, 2002, pp. 23-5.
Zhang QW, Zhang YX, Zhang Y, et al. [Determination of cirsilineol in Herba Artemisiae scopariae collected in autumn by HPLC]. Zhongguo Zhong Yao Za Zhi. 2002;27(1):23-5.
Zhang, Q. W., Zhang, Y. X., Zhang, Y., & Liang, G. G. (2002). [Determination of cirsilineol in Herba Artemisiae scopariae collected in autumn by HPLC]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 27(1), 23-5.
Zhang QW, et al. [Determination of Cirsilineol in Herba Artemisiae Scopariae Collected in Autumn By HPLC]. Zhongguo Zhong Yao Za Zhi. 2002;27(1):23-5. PubMed PMID: 12774348.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Determination of cirsilineol in Herba Artemisiae scopariae collected in autumn by HPLC]. AU - Zhang,Qi-wei, AU - Zhang,Yong-xin, AU - Zhang,Ying, AU - Liang,Guo-gang, PY - 2003/5/31/pubmed PY - 2003/9/25/medline PY - 2003/5/31/entrez SP - 23 EP - 5 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 27 IS - 1 N2 - OBJECTIVE: To establish a quantitative method for determination of cirsilineol in Herba Artemisiae Scopariae collected in Autumn. METHOD: Sample was extracted with methanol, and cleaned up with polyamide column. ODS column was used with methanol-acetonitrile-0.5% acetic acid solution (24:19:57) as mobile phase. Detection wavelength was 347 nm. RESULT: Cirsilineol in sample solution was well separated. Linearity of cirsilineol was good (r = 0.9998) in range of 0.1-0.8 microgram. The average recovery was 101.3%, RSD of repeatability was 3.04%. CONCLUSION: This method can be used for quality control of Herba Artemisiae Scopariae collected in autumn and its preparations. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/12774348/[Determination_of_cirsilineol_in_Herba_Artemisiae_scopariae_collected_in_autumn_by_HPLC]_ DB - PRIME DP - Unbound Medicine ER -