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[Isolation and elucidation of chemical constituents of shandanshaoyao decoction (II)].
Zhongguo Zhong Yao Za Zhi. 2001 Jul; 26(7):474-7.ZZ

Abstract

OBJECTIVE

To study the chemical constituents of Shandanshaoyao Decoction.

METHOD

The sample was prepared by boiling water, then precipitated by 75% of ethanol. The ethanol soluble fraction was extracted by chloroform, ethyl acetate and n-butanol, respectively. The extracts were isolated using macroreticular resin, silica gel and polyamide column chromatography, and then the chemical constituents were identified by chemical and spectroscopic methods.

RESULT

Nine compounds were isolated from the n-butanol extract and water soluble fraction, and elucidated as vitexin, quercetin, hyperoside, rutin, paeoniflorin, protocatechaldehyde, (+)-catechin, danshensu and citric acid respectively.

CONCLUSION

The chemical constituents of traditional Chinese medicinal preparations Shandanshaoyao Decoction were reported for the first time.

Authors+Show Affiliations

Institute of Materia Medica, Chinese Academy of Medical Sciences, Peking Union Medical College, Beijing 100050, China.No affiliation info available

Pub Type(s)

Journal Article

Language

chi

PubMed ID

12776360

Citation

Wen, Z M., and L X. Xu. "[Isolation and Elucidation of Chemical Constituents of Shandanshaoyao Decoction (II)]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 26, no. 7, 2001, pp. 474-7.
Wen ZM, Xu LX. [Isolation and elucidation of chemical constituents of shandanshaoyao decoction (II)]. Zhongguo Zhong Yao Za Zhi. 2001;26(7):474-7.
Wen, Z. M., & Xu, L. X. (2001). [Isolation and elucidation of chemical constituents of shandanshaoyao decoction (II)]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 26(7), 474-7.
Wen ZM, Xu LX. [Isolation and Elucidation of Chemical Constituents of Shandanshaoyao Decoction (II)]. Zhongguo Zhong Yao Za Zhi. 2001;26(7):474-7. PubMed PMID: 12776360.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Isolation and elucidation of chemical constituents of shandanshaoyao decoction (II)]. AU - Wen,Z M, AU - Xu,L X, PY - 2003/6/5/pubmed PY - 2003/10/22/medline PY - 2003/6/5/entrez SP - 474 EP - 7 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 26 IS - 7 N2 - OBJECTIVE: To study the chemical constituents of Shandanshaoyao Decoction. METHOD: The sample was prepared by boiling water, then precipitated by 75% of ethanol. The ethanol soluble fraction was extracted by chloroform, ethyl acetate and n-butanol, respectively. The extracts were isolated using macroreticular resin, silica gel and polyamide column chromatography, and then the chemical constituents were identified by chemical and spectroscopic methods. RESULT: Nine compounds were isolated from the n-butanol extract and water soluble fraction, and elucidated as vitexin, quercetin, hyperoside, rutin, paeoniflorin, protocatechaldehyde, (+)-catechin, danshensu and citric acid respectively. CONCLUSION: The chemical constituents of traditional Chinese medicinal preparations Shandanshaoyao Decoction were reported for the first time. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/12776360/[Isolation_and_elucidation_of_chemical_constituents_of_shandanshaoyao_decoction__II_]_ DB - PRIME DP - Unbound Medicine ER -