Tags

Type your tag names separated by a space and hit enter

Rugged LC-MS/MS survey analysis for acrylamide in foods.
J Agric Food Chem. 2003 Dec 17; 51(26):7547-54.JA

Abstract

The described liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the detection of acrylamide in food entails aqueous room temperature extraction, SPE cleanup, and analysis by LC-MS/MS. The method is applicable to a wide variety of foods. [(13)C(3)]acrylamide is the internal standard. The limit of quantitation is 10 ppb (microg/kg). Data were obtained in duplicate from >450 products representing >35 different food types. The variability in analyte levels in certain food types suggests that it may be possible to reduce acrylamide levels in those foods.

Authors+Show Affiliations

Center for Food Safety and Applied Nutrition, US Food and Drug Administration, 5100 Paint Branch Parkway, College Park, Maryland 20740, USA. jroach@cfsan.fda.govNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

14664505

Citation

Roach, John A G., et al. "Rugged LC-MS/MS Survey Analysis for Acrylamide in Foods." Journal of Agricultural and Food Chemistry, vol. 51, no. 26, 2003, pp. 7547-54.
Roach JA, Andrzejewski D, Gay ML, et al. Rugged LC-MS/MS survey analysis for acrylamide in foods. J Agric Food Chem. 2003;51(26):7547-54.
Roach, J. A., Andrzejewski, D., Gay, M. L., Nortrup, D., & Musser, S. M. (2003). Rugged LC-MS/MS survey analysis for acrylamide in foods. Journal of Agricultural and Food Chemistry, 51(26), 7547-54.
Roach JA, et al. Rugged LC-MS/MS Survey Analysis for Acrylamide in Foods. J Agric Food Chem. 2003 Dec 17;51(26):7547-54. PubMed PMID: 14664505.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Rugged LC-MS/MS survey analysis for acrylamide in foods. AU - Roach,John A G, AU - Andrzejewski,Denis, AU - Gay,Martha L, AU - Nortrup,David, AU - Musser,Steven M, PY - 2003/12/11/pubmed PY - 2004/1/22/medline PY - 2003/12/11/entrez SP - 7547 EP - 54 JF - Journal of agricultural and food chemistry JO - J Agric Food Chem VL - 51 IS - 26 N2 - The described liquid chromatography-tandem mass spectrometry (LC-MS/MS) method for the detection of acrylamide in food entails aqueous room temperature extraction, SPE cleanup, and analysis by LC-MS/MS. The method is applicable to a wide variety of foods. [(13)C(3)]acrylamide is the internal standard. The limit of quantitation is 10 ppb (microg/kg). Data were obtained in duplicate from >450 products representing >35 different food types. The variability in analyte levels in certain food types suggests that it may be possible to reduce acrylamide levels in those foods. SN - 0021-8561 UR - https://www.unboundmedicine.com/medline/citation/14664505/Rugged_LC_MS/MS_survey_analysis_for_acrylamide_in_foods_ L2 - https://doi.org/10.1021/jf0346354 DB - PRIME DP - Unbound Medicine ER -