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Separation and characterization of phenolic compounds in fennel (Foeniculum vulgare) using liquid chromatography-negative electrospray ionization tandem mass spectrometry.
J Agric Food Chem. 2004 Jun 16; 52(12):3679-87.JA

Abstract

Liquid chromatography (LC) diode array detection (DAD) coupled to negative electrospray ionization (ESI) tandem mass spectrometry (MS/MS) was used for the rapid and sensitive identification of water-soluble phenolic compounds in fennel waste. The plant material was first extracted and then chromatographed on Sephadex LH-20 to afford seven fractions, each of them being subjected to LC-MS analysis. Identification of the compounds was carried out by interpretation of UV, MS, and MS/MS spectra. Forty-two phenolic substances were identified, 27 of which had not previously been reported in fennel, including hydroxycinnamic acid derivatives, flavonoid glycosides, and flavonoid aglycons.

Authors+Show Affiliations

Departament de Productes Naturals, Biologia Vegetal i Edafologia, Facultat de Farmàcia, Universitat de Barcelona, Avinguda Joan XXIII s/n, 08028 Barcelona, Catalunya, Spain.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

15186082

Citation

Parejo, Irene, et al. "Separation and Characterization of Phenolic Compounds in Fennel (Foeniculum Vulgare) Using Liquid Chromatography-negative Electrospray Ionization Tandem Mass Spectrometry." Journal of Agricultural and Food Chemistry, vol. 52, no. 12, 2004, pp. 3679-87.
Parejo I, Jauregui O, Sánchez-Rabaneda F, et al. Separation and characterization of phenolic compounds in fennel (Foeniculum vulgare) using liquid chromatography-negative electrospray ionization tandem mass spectrometry. J Agric Food Chem. 2004;52(12):3679-87.
Parejo, I., Jauregui, O., Sánchez-Rabaneda, F., Viladomat, F., Bastida, J., & Codina, C. (2004). Separation and characterization of phenolic compounds in fennel (Foeniculum vulgare) using liquid chromatography-negative electrospray ionization tandem mass spectrometry. Journal of Agricultural and Food Chemistry, 52(12), 3679-87.
Parejo I, et al. Separation and Characterization of Phenolic Compounds in Fennel (Foeniculum Vulgare) Using Liquid Chromatography-negative Electrospray Ionization Tandem Mass Spectrometry. J Agric Food Chem. 2004 Jun 16;52(12):3679-87. PubMed PMID: 15186082.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Separation and characterization of phenolic compounds in fennel (Foeniculum vulgare) using liquid chromatography-negative electrospray ionization tandem mass spectrometry. AU - Parejo,Irene, AU - Jauregui,Olga, AU - Sánchez-Rabaneda,Ferran, AU - Viladomat,Francesc, AU - Bastida,Jaume, AU - Codina,Carles, PY - 2004/6/10/pubmed PY - 2004/8/4/medline PY - 2004/6/10/entrez SP - 3679 EP - 87 JF - Journal of agricultural and food chemistry JO - J Agric Food Chem VL - 52 IS - 12 N2 - Liquid chromatography (LC) diode array detection (DAD) coupled to negative electrospray ionization (ESI) tandem mass spectrometry (MS/MS) was used for the rapid and sensitive identification of water-soluble phenolic compounds in fennel waste. The plant material was first extracted and then chromatographed on Sephadex LH-20 to afford seven fractions, each of them being subjected to LC-MS analysis. Identification of the compounds was carried out by interpretation of UV, MS, and MS/MS spectra. Forty-two phenolic substances were identified, 27 of which had not previously been reported in fennel, including hydroxycinnamic acid derivatives, flavonoid glycosides, and flavonoid aglycons. SN - 0021-8561 UR - https://www.unboundmedicine.com/medline/citation/15186082/Separation_and_characterization_of_phenolic_compounds_in_fennel__Foeniculum_vulgare__using_liquid_chromatography_negative_electrospray_ionization_tandem_mass_spectrometry_ L2 - https://doi.org/10.1021/jf030813h DB - PRIME DP - Unbound Medicine ER -