Tags

Type your tag names separated by a space and hit enter

A novel double coating for microemulsion electrokinetic chromatography with laser-induced fluorescence detection: as tested with amino acid derivatives.
J Pharm Biomed Anal. 2004 Sep 21; 36(1):1-8.JP

Abstract

A novel double coating (DC) was developed for fast and reproducible microemulsion electrokinetic chromatography (MEEKC), as tested with separation and determination of amino acids using laser-induced fluorescence (LIF) detection after derivatization with 4-chloro-7-nitrobenzo-2-oxa-1,3-diazol. The simple coating is a combination of a removable covalent layer and a dynamic SDS coating. Hexamethyldisilazane was utilized for the covalent layer that can be regenerated on-line. Compared with previous no-coating method, the analysis time was shortened; and the reproducibility of migration times was improved.

Authors+Show Affiliations

Department of Chemistry, Lanzhou University, Lanzhou 730000, PR China.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

15351041

Citation

Xie, Jianping, et al. "A Novel Double Coating for Microemulsion Electrokinetic Chromatography With Laser-induced Fluorescence Detection: as Tested With Amino Acid Derivatives." Journal of Pharmaceutical and Biomedical Analysis, vol. 36, no. 1, 2004, pp. 1-8.
Xie J, Chen X, Zhang J, et al. A novel double coating for microemulsion electrokinetic chromatography with laser-induced fluorescence detection: as tested with amino acid derivatives. J Pharm Biomed Anal. 2004;36(1):1-8.
Xie, J., Chen, X., Zhang, J., Liu, J., Tian, J., Chen, X., & Hu, Z. (2004). A novel double coating for microemulsion electrokinetic chromatography with laser-induced fluorescence detection: as tested with amino acid derivatives. Journal of Pharmaceutical and Biomedical Analysis, 36(1), 1-8.
Xie J, et al. A Novel Double Coating for Microemulsion Electrokinetic Chromatography With Laser-induced Fluorescence Detection: as Tested With Amino Acid Derivatives. J Pharm Biomed Anal. 2004 Sep 21;36(1):1-8. PubMed PMID: 15351041.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - A novel double coating for microemulsion electrokinetic chromatography with laser-induced fluorescence detection: as tested with amino acid derivatives. AU - Xie,Jianping, AU - Chen,Xiaofeng, AU - Zhang,Jiyou, AU - Liu,Jiaqin, AU - Tian,Jianniao, AU - Chen,Xingguo, AU - Hu,Zhide, PY - 2004/03/08/received PY - 2004/05/12/revised PY - 2004/05/17/accepted PY - 2004/9/8/pubmed PY - 2005/2/11/medline PY - 2004/9/8/entrez SP - 1 EP - 8 JF - Journal of pharmaceutical and biomedical analysis JO - J Pharm Biomed Anal VL - 36 IS - 1 N2 - A novel double coating (DC) was developed for fast and reproducible microemulsion electrokinetic chromatography (MEEKC), as tested with separation and determination of amino acids using laser-induced fluorescence (LIF) detection after derivatization with 4-chloro-7-nitrobenzo-2-oxa-1,3-diazol. The simple coating is a combination of a removable covalent layer and a dynamic SDS coating. Hexamethyldisilazane was utilized for the covalent layer that can be regenerated on-line. Compared with previous no-coating method, the analysis time was shortened; and the reproducibility of migration times was improved. SN - 0731-7085 UR - https://www.unboundmedicine.com/medline/citation/15351041/A_novel_double_coating_for_microemulsion_electrokinetic_chromatography_with_laser_induced_fluorescence_detection:_as_tested_with_amino_acid_derivatives_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0731708504002183 DB - PRIME DP - Unbound Medicine ER -