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[Quantitative analysis of pulegone in Herba Schizonepetae].
Zhongguo Zhong Yao Za Zhi. 2005 May; 30(9):669-70.ZZ

Abstract

OBJECTIVE

To establish the determination method of pulegone in Herba Schizonepetae.

METHOD

HPLC method was developed for the determination of pulegone in Herba Schizonepetae. The separation was performed on C18 column with MeOH-H2O (80:20) as a mobile phase. The detection wavelength was set at 252 nm.

RESULT

The quantitation of pulegone in Herba Schizonepetae varied from 0.2-0.7 mg x g(-1). The average recovery is 96.2%, RSD 0.81%.

CONCLUSION

The method is simple, rapid and accurate.

Authors+Show Affiliations

Yang JP
Nanjing University of Traditional Chinese Medicine, Nanjing 210029, China.
Bao BH
No affiliation info available
Zhang L
No affiliation info available
Ding AW
No affiliation info available

MeSH

Chromatography, High Pressure LiquidCyclohexane MonoterpenesDrugs, Chinese HerbalLamiaceaeMonoterpenesPlant Components, AerialPlants, MedicinalReproducibility of Results

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

16075729

Citation

Yang, Jian-ping, et al. "[Quantitative Analysis of Pulegone in Herba Schizonepetae]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 30, no. 9, 2005, pp. 669-70.
Yang JP, Bao BH, Zhang L, et al. [Quantitative analysis of pulegone in Herba Schizonepetae]. Zhongguo Zhong Yao Za Zhi. 2005;30(9):669-70.
Yang, J. P., Bao, B. H., Zhang, L., & Ding, A. W. (2005). [Quantitative analysis of pulegone in Herba Schizonepetae]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 30(9), 669-70.
Yang JP, et al. [Quantitative Analysis of Pulegone in Herba Schizonepetae]. Zhongguo Zhong Yao Za Zhi. 2005;30(9):669-70. PubMed PMID: 16075729.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Quantitative analysis of pulegone in Herba Schizonepetae]. AU - Yang,Jian-ping, AU - Bao,Bei-hua, AU - Zhang,Li, AU - Ding,An-wei, PY - 2005/8/4/pubmed PY - 2006/5/18/medline PY - 2005/8/4/entrez SP - 669 EP - 70 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 30 IS - 9 N2 - OBJECTIVE: To establish the determination method of pulegone in Herba Schizonepetae. METHOD: HPLC method was developed for the determination of pulegone in Herba Schizonepetae. The separation was performed on C18 column with MeOH-H2O (80:20) as a mobile phase. The detection wavelength was set at 252 nm. RESULT: The quantitation of pulegone in Herba Schizonepetae varied from 0.2-0.7 mg x g(-1). The average recovery is 96.2%, RSD 0.81%. CONCLUSION: The method is simple, rapid and accurate. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/16075729/[Quantitative_analysis_of_pulegone_in_Herba_Schizonepetae]_ DB - PRIME DP - Unbound Medicine ER -