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[Analysis of volatile components from the flowers of Chrysanthemum morifolium by GC-MS with solid-phase microextraction].
Zhongguo Zhong Yao Za Zhi. 2005 Jul; 30(13):986-9.ZZ

Abstract

OBJECTIVE

To study a method for extraction and analysis of volatile components from Chrysanthemum morifolium 'gonghuangjv' cv. nov (CM GHJ) and C. morifolium 'gongbaijv' cv. nov (CM GBJ) by solid-phase microextraction (SPME) and gas chromatography-mass spectrometry (GC-MS).

METHOD

The volatile components were extracted in different temperature, different balance period and different extraction fiber using head space solid-phase microextraction (HS-SPME), and were identified by CGC-MS. The variety in integral area of each component was observed in different conditions and its relative content was determined by normalization of area.

RESULT

The better condition of SPME for C. morifolium was that the sample was extracted using 100 microm polydimethylsiloxane (PDMS) extraction fiber after it had been balanced for 6 hours at 75 degrees C. 53 components from CM GHJ and CM GBJ were identified, and there were 35 same components in CM GHJ and CM GBJ.

CONCLUSION

HS-SPME-GC-MS is convenient, rapid and reliable for analysis of volatile components in C. morifolium.

Authors+Show Affiliations

Zhou HM
Henan University of Science and Technology, Luoyang 471003, China. lyzhm@xin-huanet.com
Xie PS
No affiliation info available
Wang WH
No affiliation info available
Ma JQ
No affiliation info available
Li P
No affiliation info available

MeSH

ChrysanthemumFlowersGas Chromatography-Mass SpectrometryOils, VolatilePlants, Medicinal

Pub Type(s)

English Abstract
Journal Article

Language

chi

PubMed ID

16161424

Citation

Zhou, Hai-mei, et al. "[Analysis of Volatile Components From the Flowers of Chrysanthemum Morifolium By GC-MS With Solid-phase Microextraction]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 30, no. 13, 2005, pp. 986-9.
Zhou HM, Xie PS, Wang WH, et al. [Analysis of volatile components from the flowers of Chrysanthemum morifolium by GC-MS with solid-phase microextraction]. Zhongguo Zhong Yao Za Zhi. 2005;30(13):986-9.
Zhou, H. M., Xie, P. S., Wang, W. H., Ma, J. Q., & Li, P. (2005). [Analysis of volatile components from the flowers of Chrysanthemum morifolium by GC-MS with solid-phase microextraction]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 30(13), 986-9.
Zhou HM, et al. [Analysis of Volatile Components From the Flowers of Chrysanthemum Morifolium By GC-MS With Solid-phase Microextraction]. Zhongguo Zhong Yao Za Zhi. 2005;30(13):986-9. PubMed PMID: 16161424.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Analysis of volatile components from the flowers of Chrysanthemum morifolium by GC-MS with solid-phase microextraction]. AU - Zhou,Hai-mei, AU - Xie,Pei-shan, AU - Wang,Wan-hui, AU - Ma,Jin-qi, AU - Li,Pu, PY - 2005/9/16/pubmed PY - 2006/10/20/medline PY - 2005/9/16/entrez SP - 986 EP - 9 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 30 IS - 13 N2 - OBJECTIVE: To study a method for extraction and analysis of volatile components from Chrysanthemum morifolium 'gonghuangjv' cv. nov (CM GHJ) and C. morifolium 'gongbaijv' cv. nov (CM GBJ) by solid-phase microextraction (SPME) and gas chromatography-mass spectrometry (GC-MS). METHOD: The volatile components were extracted in different temperature, different balance period and different extraction fiber using head space solid-phase microextraction (HS-SPME), and were identified by CGC-MS. The variety in integral area of each component was observed in different conditions and its relative content was determined by normalization of area. RESULT: The better condition of SPME for C. morifolium was that the sample was extracted using 100 microm polydimethylsiloxane (PDMS) extraction fiber after it had been balanced for 6 hours at 75 degrees C. 53 components from CM GHJ and CM GBJ were identified, and there were 35 same components in CM GHJ and CM GBJ. CONCLUSION: HS-SPME-GC-MS is convenient, rapid and reliable for analysis of volatile components in C. morifolium. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/16161424/[Analysis_of_volatile_components_from_the_flowers_of_Chrysanthemum_morifolium_by_GC_MS_with_solid_phase_microextraction]_ DB - PRIME DP - Unbound Medicine ER -