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[Analysis of saponins from panax notoginseng using pressurized solvent extraction coupled with liquid chromatography-electrospray mass spectrum].
Zhong Yao Cai. 2005 Oct; 28(10):885-90.ZY

Abstract

OBJECTIVE

To establish a method for qualitative analysis of saponins from Panax notoginseng using pressurized solvent extraction coupled with LC-ESI-MS.

METHODS

The PSE technology was applied to the process of extraction for Panax notoginseng, and the negative ion detection and multiple reaction monitoring model were used. The saponins were investigated based on total ion chromatogram (TIC) and MRM chromatogram.

RESULTS

According to the fragment character of saponins, the molecular weight and their structures could be identified.

CONCLUSION

The method can be used for qualitative analysis of saponins from Panax notoginseng.

Authors+Show Affiliations

Wan J
Institute of Chinese Medical Sciences, University of Macau, Macau SAR.
Li C
No affiliation info available
Li S
No affiliation info available
Kong L
No affiliation info available
Wang Y
No affiliation info available

MeSH

Chromatography, High Pressure LiquidGinsenosidesMolecular StructureMolecular WeightPanaxPlant RootsPlants, MedicinalPressureQuality ControlSaponinsSensitivity and SpecificitySolventsSpectrometry, Mass, Electrospray IonizationTechnology, Pharmaceutical

Pub Type(s)

English Abstract
Journal Article

Language

chi

PubMed ID

16479924

Citation

Wan, Jianbo, et al. "[Analysis of Saponins From Panax Notoginseng Using Pressurized Solvent Extraction Coupled With Liquid Chromatography-electrospray Mass Spectrum]." Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, vol. 28, no. 10, 2005, pp. 885-90.
Wan J, Li C, Li S, et al. [Analysis of saponins from panax notoginseng using pressurized solvent extraction coupled with liquid chromatography-electrospray mass spectrum]. Zhong Yao Cai. 2005;28(10):885-90.
Wan, J., Li, C., Li, S., Kong, L., & Wang, Y. (2005). [Analysis of saponins from panax notoginseng using pressurized solvent extraction coupled with liquid chromatography-electrospray mass spectrum]. Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, 28(10), 885-90.
Wan J, et al. [Analysis of Saponins From Panax Notoginseng Using Pressurized Solvent Extraction Coupled With Liquid Chromatography-electrospray Mass Spectrum]. Zhong Yao Cai. 2005;28(10):885-90. PubMed PMID: 16479924.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Analysis of saponins from panax notoginseng using pressurized solvent extraction coupled with liquid chromatography-electrospray mass spectrum]. AU - Wan,Jianbo, AU - Li,Changming, AU - Li,Shaopin, AU - Kong,Lingyi, AU - Wang,Yitao, PY - 2006/2/17/pubmed PY - 2006/10/14/medline PY - 2006/2/17/entrez SP - 885 EP - 90 JF - Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials JO - Zhong Yao Cai VL - 28 IS - 10 N2 - OBJECTIVE: To establish a method for qualitative analysis of saponins from Panax notoginseng using pressurized solvent extraction coupled with LC-ESI-MS. METHODS: The PSE technology was applied to the process of extraction for Panax notoginseng, and the negative ion detection and multiple reaction monitoring model were used. The saponins were investigated based on total ion chromatogram (TIC) and MRM chromatogram. RESULTS: According to the fragment character of saponins, the molecular weight and their structures could be identified. CONCLUSION: The method can be used for qualitative analysis of saponins from Panax notoginseng. SN - 1001-4454 UR - https://www.unboundmedicine.com/medline/citation/16479924/[Analysis_of_saponins_from_panax_notoginseng_using_pressurized_solvent_extraction_coupled_with_liquid_chromatography_electrospray_mass_spectrum]_ DB - PRIME DP - Unbound Medicine ER -