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Complete 1H- and 13C NMR assignments of saponins from roots of Gypsophila trichotoma Wend.
Magn Reson Chem. 2006 Jul; 44(7):686-91.MR

Abstract

The assignments of 1H and 13C NMR spectra of two new aminoacyl triterpene saponins from roots of Gypsophila trichotoma Wend. are reported. In addition to 1D NMR methods, 2D NMR techniques (COSY, TOCSY, ROESY, HSQC, HMBC, and HSQC-TOCSY) were used for the assignments. The structures were completed by analysis of HR-ESI-MS and ESI-MS(n).

Authors+Show Affiliations

Gevrenova R
Department of Pharmacognosy, Faculty of Pharmacy, University of Medicine, 2 Dunav street, 1000 Sofia, Bulgaria.
Voutquenne-Nazabadioko L
No affiliation info available
Harakat D
No affiliation info available
Prost E
No affiliation info available
Henry M
No affiliation info available

MeSH

CaryophyllaceaeChromatography, High Pressure LiquidChromatography, Thin LayerMagnetic Resonance SpectroscopyMolecular StructurePlant RootsPlants, MedicinalSaponins

Pub Type(s)

Journal Article

Language

eng

PubMed ID

16685746

Citation

Gevrenova, Reneta, et al. "Complete 1H- and 13C NMR Assignments of Saponins From Roots of Gypsophila Trichotoma Wend." Magnetic Resonance in Chemistry : MRC, vol. 44, no. 7, 2006, pp. 686-91.
Gevrenova R, Voutquenne-Nazabadioko L, Harakat D, et al. Complete 1H- and 13C NMR assignments of saponins from roots of Gypsophila trichotoma Wend. Magn Reson Chem. 2006;44(7):686-91.
Gevrenova, R., Voutquenne-Nazabadioko, L., Harakat, D., Prost, E., & Henry, M. (2006). Complete 1H- and 13C NMR assignments of saponins from roots of Gypsophila trichotoma Wend. Magnetic Resonance in Chemistry : MRC, 44(7), 686-91.
Gevrenova R, et al. Complete 1H- and 13C NMR Assignments of Saponins From Roots of Gypsophila Trichotoma Wend. Magn Reson Chem. 2006;44(7):686-91. PubMed PMID: 16685746.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Complete 1H- and 13C NMR assignments of saponins from roots of Gypsophila trichotoma Wend. AU - Gevrenova,Reneta, AU - Voutquenne-Nazabadioko,Laurence, AU - Harakat,Dominique, AU - Prost,Elise, AU - Henry,Max, PY - 2006/5/11/pubmed PY - 2007/7/31/medline PY - 2006/5/11/entrez SP - 686 EP - 91 JF - Magnetic resonance in chemistry : MRC JO - Magn Reson Chem VL - 44 IS - 7 N2 - The assignments of 1H and 13C NMR spectra of two new aminoacyl triterpene saponins from roots of Gypsophila trichotoma Wend. are reported. In addition to 1D NMR methods, 2D NMR techniques (COSY, TOCSY, ROESY, HSQC, HMBC, and HSQC-TOCSY) were used for the assignments. The structures were completed by analysis of HR-ESI-MS and ESI-MS(n). SN - 0749-1581 UR - https://www.unboundmedicine.com/medline/citation/16685746/Complete_1H__and_13C_NMR_assignments_of_saponins_from_roots_of_Gypsophila_trichotoma_Wend_ DB - PRIME DP - Unbound Medicine ER -