Tags

Type your tag names separated by a space and hit enter

[Rapid identification of compounds in cortex moutan by liquid chromatography-tandem mass spectrometry].
Yao Xue Xue Bao. 2006 Sep; 41(9):852-6.YX

Abstract

AIM

To analyze the chemical constituents of cortex moutan by liquid chromatography coupled with electrospray ionization mass spectrometry.

METHODS

An on-line optimized HPLC-DAD/MS2 technique was employed.

RESULTS

In the negative ion detection mode, 38 components such as monoterpene glucosides, galloylglucoses and acetophenones were isolated. Among them, over thirty compounds were identified, including paeonol, paeonilflorin, oxypaeoniflorin, benzoylpaeoniflorin, benzoyloxypaeoniflorin, galloylpaeoniflorin, galloyloxypaeoniflorin, mundanpioside A, C, D, E, H, etc. by the high performance liquid chromatography with diode-array detection in parallel with electrospray ionization and quadrupole-time of flight tandem mass spectrometry (HPLC-DAD/ESI-MS2).

CONCLUSION

This method can be used to rapidly determine the constituents of cortex moutan.

Authors+Show Affiliations

Department of Pharmacognosy, China Pharmaceutical University, Nanjing 210038, China.No affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

chi

PubMed ID

17111832

Citation

Xu, Shun-jun, et al. "[Rapid Identification of Compounds in Cortex Moutan By Liquid Chromatography-tandem Mass Spectrometry]." Yao Xue Xue Bao = Acta Pharmaceutica Sinica, vol. 41, no. 9, 2006, pp. 852-6.
Xu SJ, Yang L, Zhang M, et al. [Rapid identification of compounds in cortex moutan by liquid chromatography-tandem mass spectrometry]. Yao Xue Xue Bao. 2006;41(9):852-6.
Xu, S. J., Yang, L., Zhang, M., & Wang, Z. T. (2006). [Rapid identification of compounds in cortex moutan by liquid chromatography-tandem mass spectrometry]. Yao Xue Xue Bao = Acta Pharmaceutica Sinica, 41(9), 852-6.
Xu SJ, et al. [Rapid Identification of Compounds in Cortex Moutan By Liquid Chromatography-tandem Mass Spectrometry]. Yao Xue Xue Bao. 2006;41(9):852-6. PubMed PMID: 17111832.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Rapid identification of compounds in cortex moutan by liquid chromatography-tandem mass spectrometry]. AU - Xu,Shun-jun, AU - Yang,Liu, AU - Zhang,Mian, AU - Wang,Zheng-tao, PY - 2006/11/23/pubmed PY - 2008/2/12/medline PY - 2006/11/23/entrez SP - 852 EP - 6 JF - Yao xue xue bao = Acta pharmaceutica Sinica JO - Yao Xue Xue Bao VL - 41 IS - 9 N2 - AIM: To analyze the chemical constituents of cortex moutan by liquid chromatography coupled with electrospray ionization mass spectrometry. METHODS: An on-line optimized HPLC-DAD/MS2 technique was employed. RESULTS: In the negative ion detection mode, 38 components such as monoterpene glucosides, galloylglucoses and acetophenones were isolated. Among them, over thirty compounds were identified, including paeonol, paeonilflorin, oxypaeoniflorin, benzoylpaeoniflorin, benzoyloxypaeoniflorin, galloylpaeoniflorin, galloyloxypaeoniflorin, mundanpioside A, C, D, E, H, etc. by the high performance liquid chromatography with diode-array detection in parallel with electrospray ionization and quadrupole-time of flight tandem mass spectrometry (HPLC-DAD/ESI-MS2). CONCLUSION: This method can be used to rapidly determine the constituents of cortex moutan. SN - 0513-4870 UR - https://www.unboundmedicine.com/medline/citation/17111832/[Rapid_identification_of_compounds_in_cortex_moutan_by_liquid_chromatography_tandem_mass_spectrometry]_ L2 - https://www.lens.org/lens/search/patent/list?q=citation_id:17111832 DB - PRIME DP - Unbound Medicine ER -