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[Studies on HPLC fingerprint of cortex moutan].
Zhongguo Zhong Yao Za Zhi. 2006 Oct; 31(20):1677-80.ZZ

Abstract

OBJECTIVE

To establish a HPLC fingerprint for quality evaluation of Cortex Moutan.

METHOD

The HPLC chromatographic fingerprinting of 30 lots of Cortex Moutan was established and major peaks were identified by LC-MS and MS-MS.

RESULT

The HPLC fingerprint of Cortex Moutan was established, showing 15 characteristic peaks. The areas of these peaks were found to complied with the following rule: paeonol > 1, 2, 3, 4, 6-penta-O-galloyl-glucos > methyl gallate > galloylpaeoniflorin > gallic acid > oxypaeoniflorin > other compounds.

CONCLUSION

The chromatographic fingerprinting of Cortex Moutan with high specificity can be used to control its quality and monitor lot to lot consistency.

Authors+Show Affiliations

Department of Pharmacognosy, China Pharmaceutical University, Nanjing 210038, China.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

17225532

Citation

Xu, Shun-Jun, et al. "[Studies On HPLC Fingerprint of Cortex Moutan]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 31, no. 20, 2006, pp. 1677-80.
Xu SJ, Li P, Yang L, et al. [Studies on HPLC fingerprint of cortex moutan]. Zhongguo Zhong Yao Za Zhi. 2006;31(20):1677-80.
Xu, S. J., Li, P., Yang, L., Zhang, M., & Wang, Z. T. (2006). [Studies on HPLC fingerprint of cortex moutan]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 31(20), 1677-80.
Xu SJ, et al. [Studies On HPLC Fingerprint of Cortex Moutan]. Zhongguo Zhong Yao Za Zhi. 2006;31(20):1677-80. PubMed PMID: 17225532.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Studies on HPLC fingerprint of cortex moutan]. AU - Xu,Shun-Jun, AU - Li,Peng, AU - Yang,Liu, AU - Zhang,Mian, AU - Wang,Zheng-Tao, PY - 2007/1/18/pubmed PY - 2007/12/6/medline PY - 2007/1/18/entrez SP - 1677 EP - 80 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 31 IS - 20 N2 - OBJECTIVE: To establish a HPLC fingerprint for quality evaluation of Cortex Moutan. METHOD: The HPLC chromatographic fingerprinting of 30 lots of Cortex Moutan was established and major peaks were identified by LC-MS and MS-MS. RESULT: The HPLC fingerprint of Cortex Moutan was established, showing 15 characteristic peaks. The areas of these peaks were found to complied with the following rule: paeonol > 1, 2, 3, 4, 6-penta-O-galloyl-glucos > methyl gallate > galloylpaeoniflorin > gallic acid > oxypaeoniflorin > other compounds. CONCLUSION: The chromatographic fingerprinting of Cortex Moutan with high specificity can be used to control its quality and monitor lot to lot consistency. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/17225532/[Studies_on_HPLC_fingerprint_of_cortex_moutan]_ DB - PRIME DP - Unbound Medicine ER -