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Determination of biogenic amines in squid and white prawn by high-performance liquid chromatography with postcolumn derivatization.
J Agric Food Chem. 2007 Apr 18; 55(8):3083-8.JA

Abstract

A simple method was developed for the determination of biogenic amines in aquatic food products using a reverse-phase high-performance liquid chromatography with postcolumn automatic o-phthalaldehyde derivatization and fluorescence detection. The linearity, repeatability, and recovery of the method for seven amines (tyramine, putrescine, cadaverine, histamine, agmatine, spermidine, and spermine) were evaluated. This optimized method was applied to detect biogenic amines in squid and white prawn during refrigerated storage. Sensory analysis, pH value, and total volatile base nitrogen value were combined to evaluate the freshness quality of these two raw materials. Agmatine and cadaverine in squid, cadaverine, and putrescine in white prawn were the most obviously changed amines during the storage at two different temperatures, and these biogenic amines could be the effective quality indicators for the freshness of the raw aquatic materials.

Authors+Show Affiliations

Department of Food Science and Technology, Ocean University of China, Qingdao, Shandong Province, 266003, People's Republic of China.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

17381105

Citation

Zhao, Qing-Xi, et al. "Determination of Biogenic Amines in Squid and White Prawn By High-performance Liquid Chromatography With Postcolumn Derivatization." Journal of Agricultural and Food Chemistry, vol. 55, no. 8, 2007, pp. 3083-8.
Zhao QX, Xu J, Xue CH, et al. Determination of biogenic amines in squid and white prawn by high-performance liquid chromatography with postcolumn derivatization. J Agric Food Chem. 2007;55(8):3083-8.
Zhao, Q. X., Xu, J., Xue, C. H., Sheng, W. J., Gao, R. C., Xue, Y., & Li, Z. J. (2007). Determination of biogenic amines in squid and white prawn by high-performance liquid chromatography with postcolumn derivatization. Journal of Agricultural and Food Chemistry, 55(8), 3083-8.
Zhao QX, et al. Determination of Biogenic Amines in Squid and White Prawn By High-performance Liquid Chromatography With Postcolumn Derivatization. J Agric Food Chem. 2007 Apr 18;55(8):3083-8. PubMed PMID: 17381105.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Determination of biogenic amines in squid and white prawn by high-performance liquid chromatography with postcolumn derivatization. AU - Zhao,Qing-Xi, AU - Xu,Jie, AU - Xue,Chang-Hu, AU - Sheng,Wen-Jing, AU - Gao,Rui-Chang, AU - Xue,Yong, AU - Li,Zhao-Jie, Y1 - 2007/03/24/ PY - 2007/3/27/pubmed PY - 2007/6/8/medline PY - 2007/3/27/entrez SP - 3083 EP - 8 JF - Journal of agricultural and food chemistry JO - J. Agric. Food Chem. VL - 55 IS - 8 N2 - A simple method was developed for the determination of biogenic amines in aquatic food products using a reverse-phase high-performance liquid chromatography with postcolumn automatic o-phthalaldehyde derivatization and fluorescence detection. The linearity, repeatability, and recovery of the method for seven amines (tyramine, putrescine, cadaverine, histamine, agmatine, spermidine, and spermine) were evaluated. This optimized method was applied to detect biogenic amines in squid and white prawn during refrigerated storage. Sensory analysis, pH value, and total volatile base nitrogen value were combined to evaluate the freshness quality of these two raw materials. Agmatine and cadaverine in squid, cadaverine, and putrescine in white prawn were the most obviously changed amines during the storage at two different temperatures, and these biogenic amines could be the effective quality indicators for the freshness of the raw aquatic materials. SN - 0021-8561 UR - https://www.unboundmedicine.com/medline/citation/17381105/Determination_of_biogenic_amines_in_squid_and_white_prawn_by_high_performance_liquid_chromatography_with_postcolumn_derivatization_ L2 - https://dx.doi.org/10.1021/jf062887+ DB - PRIME DP - Unbound Medicine ER -