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Simultaneous determination of 18 pyrethroids in indoor air by gas chromatography/mass spectrometry.
J Chromatogr A. 2009 Jun 26; 1216(26):5069-76.JC

Abstract

An analytical method was developed for the simultaneous measurement of 18 pyrethroids (allethrin, bifenthrin, cyfluthrin, cypermethrin, cyphenothrin, deltamethrin, empenthrin, fenpropathrin, furamethrin, imiprothrin, metofluthrin, permethrin, phenothrin, prallethrin, profluthrin, resmethrin, tetramethrin and transfluthrin) in indoor air. The pyrethroids were collected for 24 h using a combination of adsorbents (quartz fiber filter disk and Empore C18 disk), with protection from light, and then extracted with acetone, concentrated, and analyzed by GC/MS. They could be determined accurately and precisely (detection limits: ca. 1 ng/m(3)). The collected pyrethroid samples could be stored for up to one month at 4 degrees C in a refrigerator.

Authors+Show Affiliations

Osaka Prefectural Institute of Public Health, 1-3-69, Nakamichi, Higashinari-ku, Osaka 537-0025, Japan. tsyosida@iph.pref.osaka.jp

Pub Type(s)

Evaluation Study
Journal Article

Language

eng

PubMed ID

19457492

Citation

Yoshida, Toshiaki. "Simultaneous Determination of 18 Pyrethroids in Indoor Air By Gas Chromatography/mass Spectrometry." Journal of Chromatography. A, vol. 1216, no. 26, 2009, pp. 5069-76.
Yoshida T. Simultaneous determination of 18 pyrethroids in indoor air by gas chromatography/mass spectrometry. J Chromatogr A. 2009;1216(26):5069-76.
Yoshida, T. (2009). Simultaneous determination of 18 pyrethroids in indoor air by gas chromatography/mass spectrometry. Journal of Chromatography. A, 1216(26), 5069-76. https://doi.org/10.1016/j.chroma.2009.04.087
Yoshida T. Simultaneous Determination of 18 Pyrethroids in Indoor Air By Gas Chromatography/mass Spectrometry. J Chromatogr A. 2009 Jun 26;1216(26):5069-76. PubMed PMID: 19457492.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Simultaneous determination of 18 pyrethroids in indoor air by gas chromatography/mass spectrometry. A1 - Yoshida,Toshiaki, Y1 - 2009/05/03/ PY - 2009/03/23/received PY - 2009/04/23/revised PY - 2009/04/27/accepted PY - 2009/5/22/entrez PY - 2009/5/22/pubmed PY - 2009/7/25/medline SP - 5069 EP - 76 JF - Journal of chromatography. A JO - J Chromatogr A VL - 1216 IS - 26 N2 - An analytical method was developed for the simultaneous measurement of 18 pyrethroids (allethrin, bifenthrin, cyfluthrin, cypermethrin, cyphenothrin, deltamethrin, empenthrin, fenpropathrin, furamethrin, imiprothrin, metofluthrin, permethrin, phenothrin, prallethrin, profluthrin, resmethrin, tetramethrin and transfluthrin) in indoor air. The pyrethroids were collected for 24 h using a combination of adsorbents (quartz fiber filter disk and Empore C18 disk), with protection from light, and then extracted with acetone, concentrated, and analyzed by GC/MS. They could be determined accurately and precisely (detection limits: ca. 1 ng/m(3)). The collected pyrethroid samples could be stored for up to one month at 4 degrees C in a refrigerator. SN - 1873-3778 UR - https://www.unboundmedicine.com/medline/citation/19457492/Simultaneous_determination_of_18_pyrethroids_in_indoor_air_by_gas_chromatography/mass_spectrometry_ DB - PRIME DP - Unbound Medicine ER -