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Headspace solid-phase microextraction gas chromatography-mass spectrometry analysis of Eupatorium odoratum extract as an oviposition repellent.
J Chromatogr B Analyt Technol Biomed Life Sci. 2009 Jul 01; 877(20-21):1901-6.JC

Abstract

Headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS) analysis was used to study volatile and semi-volatile compounds emitted by the Eupatorium odoratum (E. odoratum) extract. Variables of HS-SPME such as the type of SPME fiber, extraction time and temperature, incubation time, desorption time and temperature have been optimized. Optimized conditions were obtained by the use of divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS) fiber, 5 min/20 min incubation/extraction time at 65 degrees C, 5 min desorption time at 260 degrees C. Using three different polar chromatographic columns to get retention index and mass spectrometry data, 99 volatile and semi-volatile compounds were tentatively identified in the E. odoratum extract. This study has identified the promising source of E. odoratum oviposition repellent.

Authors+Show Affiliations

Department of Biological Applied Engineering, Shenzhen Polytechnic, Shenzhen 518055, China. shufencui@163.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

19501027

Citation

Cui, Shufen, et al. "Headspace Solid-phase Microextraction Gas Chromatography-mass Spectrometry Analysis of Eupatorium Odoratum Extract as an Oviposition Repellent." Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, vol. 877, no. 20-21, 2009, pp. 1901-6.
Cui S, Tan S, Ouyang G, et al. Headspace solid-phase microextraction gas chromatography-mass spectrometry analysis of Eupatorium odoratum extract as an oviposition repellent. J Chromatogr B Analyt Technol Biomed Life Sci. 2009;877(20-21):1901-6.
Cui, S., Tan, S., Ouyang, G., Jiang, S., & Pawliszyn, J. (2009). Headspace solid-phase microextraction gas chromatography-mass spectrometry analysis of Eupatorium odoratum extract as an oviposition repellent. Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, 877(20-21), 1901-6. https://doi.org/10.1016/j.jchromb.2009.05.022
Cui S, et al. Headspace Solid-phase Microextraction Gas Chromatography-mass Spectrometry Analysis of Eupatorium Odoratum Extract as an Oviposition Repellent. J Chromatogr B Analyt Technol Biomed Life Sci. 2009 Jul 1;877(20-21):1901-6. PubMed PMID: 19501027.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Headspace solid-phase microextraction gas chromatography-mass spectrometry analysis of Eupatorium odoratum extract as an oviposition repellent. AU - Cui,Shufen, AU - Tan,Shuo, AU - Ouyang,Gangfeng, AU - Jiang,Shihong, AU - Pawliszyn,Janusz, Y1 - 2009/05/21/ PY - 2009/03/16/received PY - 2009/05/12/revised PY - 2009/05/12/accepted PY - 2009/6/9/entrez PY - 2009/6/9/pubmed PY - 2009/8/18/medline SP - 1901 EP - 6 JF - Journal of chromatography. B, Analytical technologies in the biomedical and life sciences JO - J Chromatogr B Analyt Technol Biomed Life Sci VL - 877 IS - 20-21 N2 - Headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS) analysis was used to study volatile and semi-volatile compounds emitted by the Eupatorium odoratum (E. odoratum) extract. Variables of HS-SPME such as the type of SPME fiber, extraction time and temperature, incubation time, desorption time and temperature have been optimized. Optimized conditions were obtained by the use of divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS) fiber, 5 min/20 min incubation/extraction time at 65 degrees C, 5 min desorption time at 260 degrees C. Using three different polar chromatographic columns to get retention index and mass spectrometry data, 99 volatile and semi-volatile compounds were tentatively identified in the E. odoratum extract. This study has identified the promising source of E. odoratum oviposition repellent. SN - 1873-376X UR - https://www.unboundmedicine.com/medline/citation/19501027/Headspace_solid_phase_microextraction_gas_chromatography_mass_spectrometry_analysis_of_Eupatorium_odoratum_extract_as_an_oviposition_repellent_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S1570-0232(09)00349-3 DB - PRIME DP - Unbound Medicine ER -