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[HPLC fingerprint of the antiarrhythmic fraction of Valeriana officinalis].
Zhong Yao Cai. 2009 Jun; 32(6):866-70.ZY

Abstract

OBJECTIVE

To establish HPLC fingerprints of the Antiarrhythmic fraction of Valeriana officinalis.

METHODS

Agilent C18 (250 mm x 4.6 mm, 5 microm) column was used and the acetonitrile-water was chosen as the mobile phase in a gradient mode. The column temperature was 380 degrees C and the detection wavelength was 218 nm. The detection time was 70 min, and the flow rate was 1.0 mL/ min.

RESULTS

Fifteen characteristic peaks were indicated in HPLC fingerprints. The relative retention time and the ranges of relative areas of the common peaks were also determined.

CONCLUSION

This method is simple and accurate with a good reproducibility and provides a reference standard for the quality control of Valeriana officinalis.

Authors+Show Affiliations

Key Laboratory of Traditional Chinese Medicine Resource and Compound Prescription, Hubei College of TCM, Ministry of Education, Wuhan 430061, China. xueyunduan@sina.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

English Abstract
Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

19764324

Citation

Duan, Xue-Yun, et al. "[HPLC Fingerprint of the Antiarrhythmic Fraction of Valeriana Officinalis]." Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, vol. 32, no. 6, 2009, pp. 866-70.
Duan XY, Gong ZF, Chen SH, et al. [HPLC fingerprint of the antiarrhythmic fraction of Valeriana officinalis]. Zhong Yao Cai. 2009;32(6):866-70.
Duan, X. Y., Gong, Z. F., Chen, S. H., Fang, Y., & Liu, Y. W. (2009). [HPLC fingerprint of the antiarrhythmic fraction of Valeriana officinalis]. Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, 32(6), 866-70.
Duan XY, et al. [HPLC Fingerprint of the Antiarrhythmic Fraction of Valeriana Officinalis]. Zhong Yao Cai. 2009;32(6):866-70. PubMed PMID: 19764324.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [HPLC fingerprint of the antiarrhythmic fraction of Valeriana officinalis]. AU - Duan,Xue-Yun, AU - Gong,Zhan-Feng, AU - Chen,Shu-He, AU - Fang,Ying, AU - Liu,Yan-Wen, PY - 2009/9/22/entrez PY - 2009/9/22/pubmed PY - 2009/12/30/medline SP - 866 EP - 70 JF - Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials JO - Zhong Yao Cai VL - 32 IS - 6 N2 - OBJECTIVE: To establish HPLC fingerprints of the Antiarrhythmic fraction of Valeriana officinalis. METHODS: Agilent C18 (250 mm x 4.6 mm, 5 microm) column was used and the acetonitrile-water was chosen as the mobile phase in a gradient mode. The column temperature was 380 degrees C and the detection wavelength was 218 nm. The detection time was 70 min, and the flow rate was 1.0 mL/ min. RESULTS: Fifteen characteristic peaks were indicated in HPLC fingerprints. The relative retention time and the ranges of relative areas of the common peaks were also determined. CONCLUSION: This method is simple and accurate with a good reproducibility and provides a reference standard for the quality control of Valeriana officinalis. SN - 1001-4454 UR - https://www.unboundmedicine.com/medline/citation/19764324/[HPLC_fingerprint_of_the_antiarrhythmic_fraction_of_Valeriana_officinalis]_ DB - PRIME DP - Unbound Medicine ER -