Tags

Type your tag names separated by a space and hit enter

Identification and quantitation of amphetamine, methamphetamine, MDMA, pseudoephedrine, and ephedrine in blood, plasma, and serum using gas chromatography-mass spectrometry (GC/MS).
Methods Mol Biol. 2010; 603:37-43.MM

Abstract

Amphetamine, methamphetamine, MDMA, pseudoephedrine, and ephedrine are measured in blood, serum, and plasma using gas chromatography coupled to mass spectrometry (GC/MS). Following a simple liquid-liquid extraction, analytes are derivatized with heptafluorobutyric anhydride (HFBA) and 1 microL injected onto a HP-5MS 15-meter capillary column. Quantitation of each analyte is accomplished using a multi-point calibration curve and deuterated internal standards. The method provides a simple, robust, and reliable means to identify and measure these analytes.

Authors+Show Affiliations

AIT Laboratories, Indianapolis, IN, USA.No affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

20077057

Citation

Gunn, Josh, et al. "Identification and Quantitation of Amphetamine, Methamphetamine, MDMA, Pseudoephedrine, and Ephedrine in Blood, Plasma, and Serum Using Gas Chromatography-mass Spectrometry (GC/MS)." Methods in Molecular Biology (Clifton, N.J.), vol. 603, 2010, pp. 37-43.
Gunn J, Kriger S, Terrell AR. Identification and quantitation of amphetamine, methamphetamine, MDMA, pseudoephedrine, and ephedrine in blood, plasma, and serum using gas chromatography-mass spectrometry (GC/MS). Methods Mol Biol. 2010;603:37-43.
Gunn, J., Kriger, S., & Terrell, A. R. (2010). Identification and quantitation of amphetamine, methamphetamine, MDMA, pseudoephedrine, and ephedrine in blood, plasma, and serum using gas chromatography-mass spectrometry (GC/MS). Methods in Molecular Biology (Clifton, N.J.), 603, 37-43. https://doi.org/10.1007/978-1-60761-459-3_4
Gunn J, Kriger S, Terrell AR. Identification and Quantitation of Amphetamine, Methamphetamine, MDMA, Pseudoephedrine, and Ephedrine in Blood, Plasma, and Serum Using Gas Chromatography-mass Spectrometry (GC/MS). Methods Mol Biol. 2010;603:37-43. PubMed PMID: 20077057.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Identification and quantitation of amphetamine, methamphetamine, MDMA, pseudoephedrine, and ephedrine in blood, plasma, and serum using gas chromatography-mass spectrometry (GC/MS). AU - Gunn,Josh, AU - Kriger,Scott, AU - Terrell,Andrea R, PY - 2010/1/16/entrez PY - 2010/1/16/pubmed PY - 2010/4/7/medline SP - 37 EP - 43 JF - Methods in molecular biology (Clifton, N.J.) JO - Methods Mol Biol VL - 603 N2 - Amphetamine, methamphetamine, MDMA, pseudoephedrine, and ephedrine are measured in blood, serum, and plasma using gas chromatography coupled to mass spectrometry (GC/MS). Following a simple liquid-liquid extraction, analytes are derivatized with heptafluorobutyric anhydride (HFBA) and 1 microL injected onto a HP-5MS 15-meter capillary column. Quantitation of each analyte is accomplished using a multi-point calibration curve and deuterated internal standards. The method provides a simple, robust, and reliable means to identify and measure these analytes. SN - 1940-6029 UR - https://www.unboundmedicine.com/medline/citation/20077057/Identification_and_quantitation_of_amphetamine_methamphetamine_MDMA_pseudoephedrine_and_ephedrine_in_blood_plasma_and_serum_using_gas_chromatography_mass_spectrometry__GC/MS__ L2 - https://dx.doi.org/10.1007/978-1-60761-459-3_4 DB - PRIME DP - Unbound Medicine ER -