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Headspace solid phase microextraction method for determination of triazine and organophosphorus pesticides in soil.
J Environ Sci Health B. 2010 Oct; 45(7):626-32.JE

Abstract

A headspace solid phase microextraction method (HS-SPME) for simultaneous determination of five pesticides belonging to triazine and organophosphorus pesticide groups in soil samples was developed. Microextraction conditions, such as temperature, extraction time and sodium chloride (NaCl) content were investigated and optimized using 100 microm polydimethyl-siloxane (PDMS) fiber. Detection and quantification were done by gas chromatography-mass spectrometry (GC-MS). Relative standard deviation (RSD) and recovery values for multiple analysis of soil samples fortified at 30 microg kg(- 1) of each pesticide were below 13 % and higher than 70 %, respectively. Limits of detection (LOD) for all the compounds studied were less than 3.2 microg kg(- 1). The proposed method was applied in the analysis of some agricultural soil samples.

Authors+Show Affiliations

Institute of Pesticides and Environmental Protection, Belgrade, Serbia. rajcica76@gmail.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Evaluation Study
Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

20803366

Citation

Durović, Rada D., et al. "Headspace Solid Phase Microextraction Method for Determination of Triazine and Organophosphorus Pesticides in Soil." Journal of Environmental Science and Health. Part. B, Pesticides, Food Contaminants, and Agricultural Wastes, vol. 45, no. 7, 2010, pp. 626-32.
Durović RD, Dorđević TM, Santrić LR, et al. Headspace solid phase microextraction method for determination of triazine and organophosphorus pesticides in soil. J Environ Sci Health B. 2010;45(7):626-32.
Durović, R. D., Dorđević, T. M., Santrić, L. R., Gasić, S. M., & Ignjatović, L. M. (2010). Headspace solid phase microextraction method for determination of triazine and organophosphorus pesticides in soil. Journal of Environmental Science and Health. Part. B, Pesticides, Food Contaminants, and Agricultural Wastes, 45(7), 626-32. https://doi.org/10.1080/03601234.2010.502416
Durović RD, et al. Headspace Solid Phase Microextraction Method for Determination of Triazine and Organophosphorus Pesticides in Soil. J Environ Sci Health B. 2010;45(7):626-32. PubMed PMID: 20803366.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Headspace solid phase microextraction method for determination of triazine and organophosphorus pesticides in soil. AU - Durović,Rada D, AU - Dorđević,Tijana M, AU - Santrić,Ljiljana R, AU - Gasić,Slavica M, AU - Ignjatović,Ljubisa M, PY - 2010/8/31/entrez PY - 2010/8/31/pubmed PY - 2010/12/14/medline SP - 626 EP - 32 JF - Journal of environmental science and health. Part. B, Pesticides, food contaminants, and agricultural wastes JO - J Environ Sci Health B VL - 45 IS - 7 N2 - A headspace solid phase microextraction method (HS-SPME) for simultaneous determination of five pesticides belonging to triazine and organophosphorus pesticide groups in soil samples was developed. Microextraction conditions, such as temperature, extraction time and sodium chloride (NaCl) content were investigated and optimized using 100 microm polydimethyl-siloxane (PDMS) fiber. Detection and quantification were done by gas chromatography-mass spectrometry (GC-MS). Relative standard deviation (RSD) and recovery values for multiple analysis of soil samples fortified at 30 microg kg(- 1) of each pesticide were below 13 % and higher than 70 %, respectively. Limits of detection (LOD) for all the compounds studied were less than 3.2 microg kg(- 1). The proposed method was applied in the analysis of some agricultural soil samples. SN - 1532-4109 UR - https://www.unboundmedicine.com/medline/citation/20803366/Headspace_solid_phase_microextraction_method_for_determination_of_triazine_and_organophosphorus_pesticides_in_soil_ L2 - http://www.tandfonline.com/doi/full/10.1080/03601234.2010.502416 DB - PRIME DP - Unbound Medicine ER -