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Selective determination of melamine in aqueous medium by molecularly imprinted solid phase extraction.
J Agric Food Chem. 2010 Nov 24; 58(22):11883-7.JA

Abstract

A molecularly imprinted polymer able to recognize melamine in partially aqueous medium was synthesized using methacrylic acid as functional monomer and ethylene glycol dimethacrylate as cross-linking agent. The bound specificity and selectivity of the obtained material were verified by performing binding experiments with melamine and its structural analogue, 2,4,6-trimethoxy-1,3,5-triazine, respectively, using different aqueous binding media. Finally, the ability of MIP to selectively extract melamine from two real samples, a food supplement and a freeze-dried meat sample, was demonstrated.

Authors+Show Affiliations

Dipartimento di Scienze Farmaceutiche, Edificio Polifunzionale, Università della Calabria, Arcavacata di Rende (CS) 87036, Italy. manuela.curcio@unical.itNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Evaluation Study
Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

20968283

Citation

Curcio, Manuela, et al. "Selective Determination of Melamine in Aqueous Medium By Molecularly Imprinted Solid Phase Extraction." Journal of Agricultural and Food Chemistry, vol. 58, no. 22, 2010, pp. 11883-7.
Curcio M, Puoci F, Cirillo G, et al. Selective determination of melamine in aqueous medium by molecularly imprinted solid phase extraction. J Agric Food Chem. 2010;58(22):11883-7.
Curcio, M., Puoci, F., Cirillo, G., Iemma, F., Spizzirri, U. G., & Picci, N. (2010). Selective determination of melamine in aqueous medium by molecularly imprinted solid phase extraction. Journal of Agricultural and Food Chemistry, 58(22), 11883-7. https://doi.org/10.1021/jf102936p
Curcio M, et al. Selective Determination of Melamine in Aqueous Medium By Molecularly Imprinted Solid Phase Extraction. J Agric Food Chem. 2010 Nov 24;58(22):11883-7. PubMed PMID: 20968283.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Selective determination of melamine in aqueous medium by molecularly imprinted solid phase extraction. AU - Curcio,Manuela, AU - Puoci,Francesco, AU - Cirillo,Giuseppe, AU - Iemma,Francesca, AU - Spizzirri,Umile Gianfranco, AU - Picci,Nevio, Y1 - 2010/10/22/ PY - 2010/10/26/entrez PY - 2010/10/26/pubmed PY - 2011/3/2/medline SP - 11883 EP - 7 JF - Journal of agricultural and food chemistry JO - J Agric Food Chem VL - 58 IS - 22 N2 - A molecularly imprinted polymer able to recognize melamine in partially aqueous medium was synthesized using methacrylic acid as functional monomer and ethylene glycol dimethacrylate as cross-linking agent. The bound specificity and selectivity of the obtained material were verified by performing binding experiments with melamine and its structural analogue, 2,4,6-trimethoxy-1,3,5-triazine, respectively, using different aqueous binding media. Finally, the ability of MIP to selectively extract melamine from two real samples, a food supplement and a freeze-dried meat sample, was demonstrated. SN - 1520-5118 UR - https://www.unboundmedicine.com/medline/citation/20968283/Selective_determination_of_melamine_in_aqueous_medium_by_molecularly_imprinted_solid_phase_extraction_ L2 - https://doi.org/10.1021/jf102936p DB - PRIME DP - Unbound Medicine ER -