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Analysis by high-performance liquid chromatography diode array detection mass spectrometry of phenolic compounds in fruit of Eucalyptus globulus cultivated in Algeria.
J Agric Food Chem. 2010 Dec 22; 58(24):12615-24.JA

Abstract

A method based on high-performance liquid chromatography coupled with diode array detection and electrospray ionization mass spectrometry (HPLC-DAD-ESI-MS) following fractionation by chromatography on a Sephadex LH-20 column has been developed to determine the phenolic composition of fruit of Eucalyptus globulus growing in Algeria. The presence of 18 gallotannins, 26 ellagitannins, and 2 flavonols was established. Tentative identification is provided for these compounds on the basis of UV-visible spectra and mass spectrometry data. Most compounds described in this study have not previously detected in fruit of E. globulus. Moreover, this is the first report of methyl digalloyl diglucose, 3,3'-O-dimethylellagic acid 4-O-β-glucopyranoside, ellagic acid hexose, methyl ellagic acid pentose, methyltetragalloylglucose, and valoneic acid isomers (sanguisorbic, flavogallic acid dilactone) in the genus Eucalyptus. Quantitatively, ellagic acid and its derivatives, including ellagitannins, are largely predominant.

Authors+Show Affiliations

Faculty of Nature and Life Sciences, 3bs Laboratory, A. Mira University, Bejaia 06000, Algeria.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Evaluation Study
Journal Article

Language

eng

PubMed ID

21121679

Citation

Boulekbache-Makhlouf, Lila, et al. "Analysis By High-performance Liquid Chromatography Diode Array Detection Mass Spectrometry of Phenolic Compounds in Fruit of Eucalyptus Globulus Cultivated in Algeria." Journal of Agricultural and Food Chemistry, vol. 58, no. 24, 2010, pp. 12615-24.
Boulekbache-Makhlouf L, Meudec E, Chibane M, et al. Analysis by high-performance liquid chromatography diode array detection mass spectrometry of phenolic compounds in fruit of Eucalyptus globulus cultivated in Algeria. J Agric Food Chem. 2010;58(24):12615-24.
Boulekbache-Makhlouf, L., Meudec, E., Chibane, M., Mazauric, J. P., Slimani, S., Henry, M., Cheynier, V., & Madani, K. (2010). Analysis by high-performance liquid chromatography diode array detection mass spectrometry of phenolic compounds in fruit of Eucalyptus globulus cultivated in Algeria. Journal of Agricultural and Food Chemistry, 58(24), 12615-24. https://doi.org/10.1021/jf1029509
Boulekbache-Makhlouf L, et al. Analysis By High-performance Liquid Chromatography Diode Array Detection Mass Spectrometry of Phenolic Compounds in Fruit of Eucalyptus Globulus Cultivated in Algeria. J Agric Food Chem. 2010 Dec 22;58(24):12615-24. PubMed PMID: 21121679.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Analysis by high-performance liquid chromatography diode array detection mass spectrometry of phenolic compounds in fruit of Eucalyptus globulus cultivated in Algeria. AU - Boulekbache-Makhlouf,Lila, AU - Meudec,Emmanuelle, AU - Chibane,Mohamed, AU - Mazauric,Jean-Paul, AU - Slimani,Sakina, AU - Henry,Max, AU - Cheynier,Veronique, AU - Madani,Khodir, Y1 - 2010/12/01/ PY - 2010/12/3/entrez PY - 2010/12/3/pubmed PY - 2011/3/24/medline SP - 12615 EP - 24 JF - Journal of agricultural and food chemistry JO - J Agric Food Chem VL - 58 IS - 24 N2 - A method based on high-performance liquid chromatography coupled with diode array detection and electrospray ionization mass spectrometry (HPLC-DAD-ESI-MS) following fractionation by chromatography on a Sephadex LH-20 column has been developed to determine the phenolic composition of fruit of Eucalyptus globulus growing in Algeria. The presence of 18 gallotannins, 26 ellagitannins, and 2 flavonols was established. Tentative identification is provided for these compounds on the basis of UV-visible spectra and mass spectrometry data. Most compounds described in this study have not previously detected in fruit of E. globulus. Moreover, this is the first report of methyl digalloyl diglucose, 3,3'-O-dimethylellagic acid 4-O-β-glucopyranoside, ellagic acid hexose, methyl ellagic acid pentose, methyltetragalloylglucose, and valoneic acid isomers (sanguisorbic, flavogallic acid dilactone) in the genus Eucalyptus. Quantitatively, ellagic acid and its derivatives, including ellagitannins, are largely predominant. SN - 1520-5118 UR - https://www.unboundmedicine.com/medline/citation/21121679/Analysis_by_high_performance_liquid_chromatography_diode_array_detection_mass_spectrometry_of_phenolic_compounds_in_fruit_of_Eucalyptus_globulus_cultivated_in_Algeria_ L2 - https://doi.org/10.1021/jf1029509 DB - PRIME DP - Unbound Medicine ER -