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Optimization of the extraction conditions of the volatile compounds from chili peppers by headspace solid phase micro-extraction.
J Chromatogr A. 2011 May 27; 1218(21):3345-50.JC

Abstract

A method involving headspace-solid phase micro-extraction (HS-SPME), gas chromatography with flame ionization detection (GC-FID) and gas chromatography with mass spectrometry (GC-MS) was developed and optimized to investigate the volatile composition of Capsicum chili peppers. Five SPME fibers were tested for extraction: carboxen/polydimethylsiloxane (CAR/PDMS-75μm), polydimethylsiloxane (PDMS-100μm), divinylbenzene/polydimethylsiloxane (DVB/PDMS-65μm), carbowax/divinylbenzene (CW/DVB-70μm), and divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS-50/30μm), the last of which was shown to be the most efficient fiber to trap the volatile compounds. Optimization of the extraction conditions was carried out using multivariate strategies such as factorial design and response surface methodology. Eighty three compounds were identified by GC-MS when using the optimized extraction conditions, the majority of which were esters.

Authors+Show Affiliations

Department of Food Science, Faculty of Food Engineering, Campinas State University, Campinas, SP, Brazil.No affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

21227437

Citation

Junior, Stanislau Bogusz, et al. "Optimization of the Extraction Conditions of the Volatile Compounds From Chili Peppers By Headspace Solid Phase Micro-extraction." Journal of Chromatography. A, vol. 1218, no. 21, 2011, pp. 3345-50.
Junior SB, de Marchi Tavares de Melo A, Zini CA, et al. Optimization of the extraction conditions of the volatile compounds from chili peppers by headspace solid phase micro-extraction. J Chromatogr A. 2011;1218(21):3345-50.
Junior, S. B., de Marchi Tavares de Melo, A., Zini, C. A., & Godoy, H. T. (2011). Optimization of the extraction conditions of the volatile compounds from chili peppers by headspace solid phase micro-extraction. Journal of Chromatography. A, 1218(21), 3345-50. https://doi.org/10.1016/j.chroma.2010.12.060
Junior SB, et al. Optimization of the Extraction Conditions of the Volatile Compounds From Chili Peppers By Headspace Solid Phase Micro-extraction. J Chromatogr A. 2011 May 27;1218(21):3345-50. PubMed PMID: 21227437.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Optimization of the extraction conditions of the volatile compounds from chili peppers by headspace solid phase micro-extraction. AU - Junior,Stanislau Bogusz, AU - de Marchi Tavares de Melo,Arlete, AU - Zini,Cláudia Alcaraz, AU - Godoy,Helena Teixeira, Y1 - 2010/12/21/ PY - 2010/08/25/received PY - 2010/12/07/revised PY - 2010/12/14/accepted PY - 2011/1/14/entrez PY - 2011/1/14/pubmed PY - 2011/8/11/medline SP - 3345 EP - 50 JF - Journal of chromatography. A JO - J Chromatogr A VL - 1218 IS - 21 N2 - A method involving headspace-solid phase micro-extraction (HS-SPME), gas chromatography with flame ionization detection (GC-FID) and gas chromatography with mass spectrometry (GC-MS) was developed and optimized to investigate the volatile composition of Capsicum chili peppers. Five SPME fibers were tested for extraction: carboxen/polydimethylsiloxane (CAR/PDMS-75μm), polydimethylsiloxane (PDMS-100μm), divinylbenzene/polydimethylsiloxane (DVB/PDMS-65μm), carbowax/divinylbenzene (CW/DVB-70μm), and divinylbenzene/carboxen/polydimethylsiloxane (DVB/CAR/PDMS-50/30μm), the last of which was shown to be the most efficient fiber to trap the volatile compounds. Optimization of the extraction conditions was carried out using multivariate strategies such as factorial design and response surface methodology. Eighty three compounds were identified by GC-MS when using the optimized extraction conditions, the majority of which were esters. SN - 1873-3778 UR - https://www.unboundmedicine.com/medline/citation/21227437/Optimization_of_the_extraction_conditions_of_the_volatile_compounds_from_chili_peppers_by_headspace_solid_phase_micro_extraction_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0021-9673(10)01752-8 DB - PRIME DP - Unbound Medicine ER -