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Development of an ionic liquid-based ultrasonic-assisted liquid-liquid microextraction method for sensitive determination of biogenic amines: application to the analysis of octopamine, tyramine and phenethylamine in beer samples.
J Chromatogr B Analyt Technol Biomed Life Sci. 2011 Mar 15; 879(9-10):579-84.JC

Abstract

A simple and efficient method, ionic liquid-based ultrasound-assisted liquid-liquid microextraction, has been developed for the determination of three biogenic amines including octopamine (OCT), tyramine (TYR) and phenethylamine (PHE). Fluorescence probe 2,6-dimethyl-4-quinolinecarboxylic acid N-hydroxysuccinimide ester was applied for derivatization of biogenic amines and high-performance liquid chromatography coupled with fluorescence detection was used for the determination of the derivatives. The factors affecting the extraction efficiency, such as the type and volume of ionic liquid, ultrasonication time and centrifugation time have been investigated in detail. Under the optimum conditions, linearity of the method was observed in the range of 0.5-50 μgmL(-1) for OCT and TYR, and 0.025-2.5 μgmL(-1) for PHE, respectively, with correlation coefficients (γ)>0.996. The limits of detection ranged from 0.25-50 ngmL(-1) (S/N=3). The spiked recoveries of three target compounds in beer samples were in the range of 90.2-114%. As a result, this method has been successfully applied for the sensitive determination of OCT, TYR and PHE in beer samples.

Authors+Show Affiliations

College of Chemistry and Chemical Engineering, Xinyang Normal University, Xinyang 464000, PR China. kejinghuang@163.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

21316314

Citation

Huang, Ke-Jing, et al. "Development of an Ionic Liquid-based Ultrasonic-assisted Liquid-liquid Microextraction Method for Sensitive Determination of Biogenic Amines: Application to the Analysis of Octopamine, Tyramine and Phenethylamine in Beer Samples." Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, vol. 879, no. 9-10, 2011, pp. 579-84.
Huang KJ, Jin CX, Song SL, et al. Development of an ionic liquid-based ultrasonic-assisted liquid-liquid microextraction method for sensitive determination of biogenic amines: application to the analysis of octopamine, tyramine and phenethylamine in beer samples. J Chromatogr B Analyt Technol Biomed Life Sci. 2011;879(9-10):579-84.
Huang, K. J., Jin, C. X., Song, S. L., Wei, C. Y., Liu, Y. M., & Li, J. (2011). Development of an ionic liquid-based ultrasonic-assisted liquid-liquid microextraction method for sensitive determination of biogenic amines: application to the analysis of octopamine, tyramine and phenethylamine in beer samples. Journal of Chromatography. B, Analytical Technologies in the Biomedical and Life Sciences, 879(9-10), 579-84. https://doi.org/10.1016/j.jchromb.2011.01.018
Huang KJ, et al. Development of an Ionic Liquid-based Ultrasonic-assisted Liquid-liquid Microextraction Method for Sensitive Determination of Biogenic Amines: Application to the Analysis of Octopamine, Tyramine and Phenethylamine in Beer Samples. J Chromatogr B Analyt Technol Biomed Life Sci. 2011 Mar 15;879(9-10):579-84. PubMed PMID: 21316314.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Development of an ionic liquid-based ultrasonic-assisted liquid-liquid microextraction method for sensitive determination of biogenic amines: application to the analysis of octopamine, tyramine and phenethylamine in beer samples. AU - Huang,Ke-Jing, AU - Jin,Chun-Xue, AU - Song,Shi-Lin, AU - Wei,Cai-Yun, AU - Liu,Yan-Ming, AU - Li,Jing, Y1 - 2011/01/27/ PY - 2010/04/05/received PY - 2011/01/15/revised PY - 2011/01/18/accepted PY - 2011/2/15/entrez PY - 2011/2/15/pubmed PY - 2011/7/1/medline SP - 579 EP - 84 JF - Journal of chromatography. B, Analytical technologies in the biomedical and life sciences JO - J. Chromatogr. B Analyt. Technol. Biomed. Life Sci. VL - 879 IS - 9-10 N2 - A simple and efficient method, ionic liquid-based ultrasound-assisted liquid-liquid microextraction, has been developed for the determination of three biogenic amines including octopamine (OCT), tyramine (TYR) and phenethylamine (PHE). Fluorescence probe 2,6-dimethyl-4-quinolinecarboxylic acid N-hydroxysuccinimide ester was applied for derivatization of biogenic amines and high-performance liquid chromatography coupled with fluorescence detection was used for the determination of the derivatives. The factors affecting the extraction efficiency, such as the type and volume of ionic liquid, ultrasonication time and centrifugation time have been investigated in detail. Under the optimum conditions, linearity of the method was observed in the range of 0.5-50 μgmL(-1) for OCT and TYR, and 0.025-2.5 μgmL(-1) for PHE, respectively, with correlation coefficients (γ)>0.996. The limits of detection ranged from 0.25-50 ngmL(-1) (S/N=3). The spiked recoveries of three target compounds in beer samples were in the range of 90.2-114%. As a result, this method has been successfully applied for the sensitive determination of OCT, TYR and PHE in beer samples. SN - 1873-376X UR - https://www.unboundmedicine.com/medline/citation/21316314/Development_of_an_ionic_liquid_based_ultrasonic_assisted_liquid_liquid_microextraction_method_for_sensitive_determination_of_biogenic_amines:_application_to_the_analysis_of_octopamine_tyramine_and_phenethylamine_in_beer_samples_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S1570-0232(11)00052-3 DB - PRIME DP - Unbound Medicine ER -