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Anodized aluminum wire as a solid-phase microextraction fiber for rapid determination of volatile constituents in medicinal plant.
Anal Chim Acta. 2011 Sep 02; 701(1):1-5.AC

Abstract

Headspace solid phase microextraction using anodized aluminum fiber in combination with capillary GC-MS was utilized as monitoring technique for the collection and detection of the volatile compounds of Echinophora platyloba DC. Experimental parameters, including the sample weight, extraction temperature, extraction time and humidity effect, desorption time and desorption temperature were examined and optimized. Using HS-SPME followed by GC-MS, 53 compounds were separated and identified in E. platyloba DC, which mainly included E-β ocimene (47.63%), R-D-decalactone (13.28%), α-pinene (7.43%) and nonane (6.71%). Compared with hydrodistillation (HD), HS-SPME, provides the advantages of a small amount of sample, timesaving, simplicity and cheapness. To the best of our knowledge, this is the first report on using anodized aluminum fiber in solid-phase microextraction coupled to headspace for the investigation of volatile fraction of medicinal plant.

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Authors+Show Affiliations

Gholivand MB
Department of Analytical Chemistry, Faculty of Chemistry, Razi University, Kermanshah, Iran. mbgholivand@yahoo.com
Piryaei M
No affiliation info available
Abolghasemi MM
No affiliation info available

MeSH

AluminumElectrodesEquipment DesignGas Chromatography-Mass SpectrometryHumidityOils, VolatilePlant ExtractsPlants, MedicinalSolid Phase MicroextractionVolatile Organic Compounds

Pub Type(s)

Evaluation Study
Journal Article

Language

eng

PubMed ID

21763801

Citation

Gholivand, Mohammad Bagher, et al. "Anodized Aluminum Wire as a Solid-phase Microextraction Fiber for Rapid Determination of Volatile Constituents in Medicinal Plant." Analytica Chimica Acta, vol. 701, no. 1, 2011, pp. 1-5.
Gholivand MB, Piryaei M, Abolghasemi MM. Anodized aluminum wire as a solid-phase microextraction fiber for rapid determination of volatile constituents in medicinal plant. Anal Chim Acta. 2011;701(1):1-5.
Gholivand, M. B., Piryaei, M., & Abolghasemi, M. M. (2011). Anodized aluminum wire as a solid-phase microextraction fiber for rapid determination of volatile constituents in medicinal plant. Analytica Chimica Acta, 701(1), 1-5. https://doi.org/10.1016/j.aca.2011.05.046
Gholivand MB, Piryaei M, Abolghasemi MM. Anodized Aluminum Wire as a Solid-phase Microextraction Fiber for Rapid Determination of Volatile Constituents in Medicinal Plant. Anal Chim Acta. 2011 Sep 2;701(1):1-5. PubMed PMID: 21763801.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Anodized aluminum wire as a solid-phase microextraction fiber for rapid determination of volatile constituents in medicinal plant. AU - Gholivand,Mohammad Bagher, AU - Piryaei,Marzieh, AU - Abolghasemi,Mir Mahdi, Y1 - 2011/06/02/ PY - 2011/02/18/received PY - 2011/05/24/revised PY - 2011/05/27/accepted PY - 2011/7/19/entrez PY - 2011/7/19/pubmed PY - 2011/11/2/medline SP - 1 EP - 5 JF - Analytica chimica acta JO - Anal Chim Acta VL - 701 IS - 1 N2 - Headspace solid phase microextraction using anodized aluminum fiber in combination with capillary GC-MS was utilized as monitoring technique for the collection and detection of the volatile compounds of Echinophora platyloba DC. Experimental parameters, including the sample weight, extraction temperature, extraction time and humidity effect, desorption time and desorption temperature were examined and optimized. Using HS-SPME followed by GC-MS, 53 compounds were separated and identified in E. platyloba DC, which mainly included E-β ocimene (47.63%), R-D-decalactone (13.28%), α-pinene (7.43%) and nonane (6.71%). Compared with hydrodistillation (HD), HS-SPME, provides the advantages of a small amount of sample, timesaving, simplicity and cheapness. To the best of our knowledge, this is the first report on using anodized aluminum fiber in solid-phase microextraction coupled to headspace for the investigation of volatile fraction of medicinal plant. SN - 1873-4324 UR - https://www.unboundmedicine.com/medline/citation/21763801/Anodized_aluminum_wire_as_a_solid_phase_microextraction_fiber_for_rapid_determination_of_volatile_constituents_in_medicinal_plant_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0003-2670(11)00764-1 DB - PRIME DP - Unbound Medicine ER -