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Preparation and evaluation of molecularly imprinted ionic liquids polymer as sorbent for on-line solid-phase extraction of chlorsulfuron in environmental water samples.
J Chromatogr A. 2011 Sep 16; 1218(37):6271-7.JC

Abstract

In this report, vinylimidazolium ionic liquid as a functional monomer for preparation of chlorsulfuron (CS) imprinted polymers were first studied. The imprinted materials showed high selectivity for CS, and fast kinetics so that adsorption equilibrium was achieved within 5 min. These materials have been further employed to detect trace CS from water samples by online preconcentration coupled with HPLC. The sorbent offered good linearity (0.005-30 μg L(-1), r(2)>0.99) for on-line solid-phase extraction of trace chlorsulfuron. Under the optimal experimental conditions, the recovery for chlorsulfuron was in the range of 81.0-110.1% for the water samples, with RSDs ranging from 1.2 to 7.6%.

Authors+Show Affiliations

Key Laboratory of Food Nutrition and Safety, Ministry of Education of China, Tianjin University of Science and Technology, Tianjin 300457, China.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

21807367

Citation

Guo, Lu, et al. "Preparation and Evaluation of Molecularly Imprinted Ionic Liquids Polymer as Sorbent for On-line Solid-phase Extraction of Chlorsulfuron in Environmental Water Samples." Journal of Chromatography. A, vol. 1218, no. 37, 2011, pp. 6271-7.
Guo L, Deng Q, Fang G, et al. Preparation and evaluation of molecularly imprinted ionic liquids polymer as sorbent for on-line solid-phase extraction of chlorsulfuron in environmental water samples. J Chromatogr A. 2011;1218(37):6271-7.
Guo, L., Deng, Q., Fang, G., Gao, W., & Wang, S. (2011). Preparation and evaluation of molecularly imprinted ionic liquids polymer as sorbent for on-line solid-phase extraction of chlorsulfuron in environmental water samples. Journal of Chromatography. A, 1218(37), 6271-7. https://doi.org/10.1016/j.chroma.2011.07.016
Guo L, et al. Preparation and Evaluation of Molecularly Imprinted Ionic Liquids Polymer as Sorbent for On-line Solid-phase Extraction of Chlorsulfuron in Environmental Water Samples. J Chromatogr A. 2011 Sep 16;1218(37):6271-7. PubMed PMID: 21807367.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Preparation and evaluation of molecularly imprinted ionic liquids polymer as sorbent for on-line solid-phase extraction of chlorsulfuron in environmental water samples. AU - Guo,Lu, AU - Deng,Qiliang, AU - Fang,Guozhen, AU - Gao,Wei, AU - Wang,Shuo, Y1 - 2011/07/20/ PY - 2010/12/31/received PY - 2011/06/20/revised PY - 2011/07/08/accepted PY - 2011/8/3/entrez PY - 2011/8/3/pubmed PY - 2011/10/25/medline SP - 6271 EP - 7 JF - Journal of chromatography. A JO - J Chromatogr A VL - 1218 IS - 37 N2 - In this report, vinylimidazolium ionic liquid as a functional monomer for preparation of chlorsulfuron (CS) imprinted polymers were first studied. The imprinted materials showed high selectivity for CS, and fast kinetics so that adsorption equilibrium was achieved within 5 min. These materials have been further employed to detect trace CS from water samples by online preconcentration coupled with HPLC. The sorbent offered good linearity (0.005-30 μg L(-1), r(2)>0.99) for on-line solid-phase extraction of trace chlorsulfuron. Under the optimal experimental conditions, the recovery for chlorsulfuron was in the range of 81.0-110.1% for the water samples, with RSDs ranging from 1.2 to 7.6%. SN - 1873-3778 UR - https://www.unboundmedicine.com/medline/citation/21807367/Preparation_and_evaluation_of_molecularly_imprinted_ionic_liquids_polymer_as_sorbent_for_on_line_solid_phase_extraction_of_chlorsulfuron_in_environmental_water_samples_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0021-9673(11)01006-5 DB - PRIME DP - Unbound Medicine ER -