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Aroma evaluation of gamazumi (Viburnum dilatatum) by aroma extract dilution analysis and odour activity value.
Phytochem Anal. 2012 May-Jun; 23(3):208-13.PA

Abstract

INTRODUCTION

Viburnum dilatatum (gamazumi) is widely distributed in Japan and China. Recently, juice from V. dilatatum fruits has been manufactured in Japan. Concerning the aroma of V. dilatatum, phenethyl alcohol, 3Z-hexenol and l-linalool have been identified in the essential oil from the flowers of V. dilatatum, however, there are no detailed reports on the aroma of V. dilatatum elucidated using sensory evaluation.

OBJECTIVE

To clarify odourants contributing to the characteristic aroma, the aroma extract dilution analysis (AEDA) method was performed through gas chromatography olfactometry (GC-O) analysis.

METHODOLOGY

The aroma-active compounds were identified by GC-O and AEDA, and in order to determine the relative contribution of each compound to the aroma of V. dilatatum, odour activity value (OAV) has been used.

RESULTS

The hydrodistillation of the leaf and branch of V. dilatatum afforded pale yellowish oils, with yields of 0.008 and 0.015% (w/w). The main components of the leaf oil were 3Z-hexenal (12.7%) and linalool (10.8%). In branch oil, palmitic acid (18.3%) and linoleic acid (8.2%) were identified. With regard to aroma components, 24 and 14 compounds were identified in the leaf and branch oils respectively, by GC-O analysis.

CONCLUSION

On the basis of AEDA, OAVs and sensory evaluations, nonanal is estimated as the main aroma compound of leaf and branch oil, as the other aroma compounds, C₆ compounds and 2-pentyl furan make green odour; linalool, eugenol and β-ionone play important role in the sweet odour of leaf oil. In branch oil, cis-furanlinalool oxide and eugenol make sweet odour, and β-eudesmol contributes to woody odour.

Authors+Show Affiliations

Department of Applied Chemistry, Faculty of Science and Engineering, Kinki University, 3-4-1 Kowakae, Higashiosaka-shi, Osaka 577-8502, Japan. miyazawa@apch.kindai.ac.jpNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article

Language

eng

PubMed ID

21858881

Citation

Miyazawa, Mitsuo, et al. "Aroma Evaluation of Gamazumi (Viburnum Dilatatum) By Aroma Extract Dilution Analysis and Odour Activity Value." Phytochemical Analysis : PCA, vol. 23, no. 3, 2012, pp. 208-13.
Miyazawa M, Hashidume S, Takahashi T, et al. Aroma evaluation of gamazumi (Viburnum dilatatum) by aroma extract dilution analysis and odour activity value. Phytochem Anal. 2012;23(3):208-13.
Miyazawa, M., Hashidume, S., Takahashi, T., & Kikuchi, T. (2012). Aroma evaluation of gamazumi (Viburnum dilatatum) by aroma extract dilution analysis and odour activity value. Phytochemical Analysis : PCA, 23(3), 208-13. https://doi.org/10.1002/pca.1344
Miyazawa M, et al. Aroma Evaluation of Gamazumi (Viburnum Dilatatum) By Aroma Extract Dilution Analysis and Odour Activity Value. Phytochem Anal. 2012 May-Jun;23(3):208-13. PubMed PMID: 21858881.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Aroma evaluation of gamazumi (Viburnum dilatatum) by aroma extract dilution analysis and odour activity value. AU - Miyazawa,Mitsuo, AU - Hashidume,Shunsuke, AU - Takahashi,Toshiyuki, AU - Kikuchi,Tohru, Y1 - 2011/08/21/ PY - 2011/03/14/received PY - 2011/05/11/revised PY - 2011/05/20/accepted PY - 2011/8/23/entrez PY - 2011/8/23/pubmed PY - 2012/8/14/medline SP - 208 EP - 13 JF - Phytochemical analysis : PCA JO - Phytochem Anal VL - 23 IS - 3 N2 - INTRODUCTION: Viburnum dilatatum (gamazumi) is widely distributed in Japan and China. Recently, juice from V. dilatatum fruits has been manufactured in Japan. Concerning the aroma of V. dilatatum, phenethyl alcohol, 3Z-hexenol and l-linalool have been identified in the essential oil from the flowers of V. dilatatum, however, there are no detailed reports on the aroma of V. dilatatum elucidated using sensory evaluation. OBJECTIVE: To clarify odourants contributing to the characteristic aroma, the aroma extract dilution analysis (AEDA) method was performed through gas chromatography olfactometry (GC-O) analysis. METHODOLOGY: The aroma-active compounds were identified by GC-O and AEDA, and in order to determine the relative contribution of each compound to the aroma of V. dilatatum, odour activity value (OAV) has been used. RESULTS: The hydrodistillation of the leaf and branch of V. dilatatum afforded pale yellowish oils, with yields of 0.008 and 0.015% (w/w). The main components of the leaf oil were 3Z-hexenal (12.7%) and linalool (10.8%). In branch oil, palmitic acid (18.3%) and linoleic acid (8.2%) were identified. With regard to aroma components, 24 and 14 compounds were identified in the leaf and branch oils respectively, by GC-O analysis. CONCLUSION: On the basis of AEDA, OAVs and sensory evaluations, nonanal is estimated as the main aroma compound of leaf and branch oil, as the other aroma compounds, C₆ compounds and 2-pentyl furan make green odour; linalool, eugenol and β-ionone play important role in the sweet odour of leaf oil. In branch oil, cis-furanlinalool oxide and eugenol make sweet odour, and β-eudesmol contributes to woody odour. SN - 1099-1565 UR - https://www.unboundmedicine.com/medline/citation/21858881/Aroma_evaluation_of_gamazumi__Viburnum_dilatatum__by_aroma_extract_dilution_analysis_and_odour_activity_value_ L2 - https://doi.org/10.1002/pca.1344 DB - PRIME DP - Unbound Medicine ER -