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[Determination of content changes of three diester-diterpenoid alkaloids in compatibility of radix aconiti laterlis preparata and Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Radix ampelopsis, Rhizoma bletillae by HPLC].
Zhong Yao Cai. 2011 Dec; 34(12):1891-4.ZY

Abstract

OBJECTIVE

To analyze the three diester-alkaloids content in the decoctions before and after Radix aconiti lateralis preparata combined with Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Radix ampelopsis, Rhizoma bletillae, respectively.

METHODS

HPLC analysis was performed on a Agilent Extend C18 column,eluted with a mobile phase consisted of acetonitrile/methanol - 35 mmol/L ammonium acetate and gradient elution,with a flow rate of 0.6 ml/min and the detection wavelength of 235 nm.

RESULTS

The contents of three diester-alkaloids in the co-decoctions of Radix aconiti laterlis preparata combined with Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Rhizoma bletillae were more than that of single Radix aconiti laterlis preparata decoction, expect the Bulbus fritillariae cirrhosae,Radix ampelopsis and Rhizoma pinelliae praeparatum. From the result,we can found that the content of three diester-alkaloids in decoctions was correlated with the decoction pH.

CONCLUSION

The pH of decoction is one of the most important factors to relate the three diester-alkaloids content in the decoctions.

Authors+Show Affiliations

Changchun University of Traditional Chinese Medicine, Changchun 130117, China. dongxin.16@163.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

22500426

Citation

Dong, Xin, et al. "[Determination of Content Changes of Three Diester-diterpenoid Alkaloids in Compatibility of Radix Aconiti Laterlis Preparata and Rhizoma Pinelliae, Fructus Trichosanthis, Bulbus Fritillariae, Radix Ampelopsis, Rhizoma Bletillae By HPLC]." Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, vol. 34, no. 12, 2011, pp. 1891-4.
Dong X, Wang SM, Li XM, et al. [Determination of content changes of three diester-diterpenoid alkaloids in compatibility of radix aconiti laterlis preparata and Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Radix ampelopsis, Rhizoma bletillae by HPLC]. Zhong Yao Cai. 2011;34(12):1891-4.
Dong, X., Wang, S. M., Li, X. M., Song, F. R., Liu, Z. Q., & Liu, S. Y. (2011). [Determination of content changes of three diester-diterpenoid alkaloids in compatibility of radix aconiti laterlis preparata and Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Radix ampelopsis, Rhizoma bletillae by HPLC]. Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, 34(12), 1891-4.
Dong X, et al. [Determination of Content Changes of Three Diester-diterpenoid Alkaloids in Compatibility of Radix Aconiti Laterlis Preparata and Rhizoma Pinelliae, Fructus Trichosanthis, Bulbus Fritillariae, Radix Ampelopsis, Rhizoma Bletillae By HPLC]. Zhong Yao Cai. 2011;34(12):1891-4. PubMed PMID: 22500426.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Determination of content changes of three diester-diterpenoid alkaloids in compatibility of radix aconiti laterlis preparata and Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Radix ampelopsis, Rhizoma bletillae by HPLC]. AU - Dong,Xin, AU - Wang,Shu-Min, AU - Li,Xiao-Ming, AU - Song,Feng-Rui, AU - Liu,Zhi-Qiang, AU - Liu,Shu-Ying, PY - 2012/4/17/entrez PY - 2012/4/17/pubmed PY - 2012/9/21/medline SP - 1891 EP - 4 JF - Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials JO - Zhong Yao Cai VL - 34 IS - 12 N2 - OBJECTIVE: To analyze the three diester-alkaloids content in the decoctions before and after Radix aconiti lateralis preparata combined with Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Radix ampelopsis, Rhizoma bletillae, respectively. METHODS: HPLC analysis was performed on a Agilent Extend C18 column,eluted with a mobile phase consisted of acetonitrile/methanol - 35 mmol/L ammonium acetate and gradient elution,with a flow rate of 0.6 ml/min and the detection wavelength of 235 nm. RESULTS: The contents of three diester-alkaloids in the co-decoctions of Radix aconiti laterlis preparata combined with Rhizoma pinelliae, Fructus trichosanthis, Bulbus fritillariae, Rhizoma bletillae were more than that of single Radix aconiti laterlis preparata decoction, expect the Bulbus fritillariae cirrhosae,Radix ampelopsis and Rhizoma pinelliae praeparatum. From the result,we can found that the content of three diester-alkaloids in decoctions was correlated with the decoction pH. CONCLUSION: The pH of decoction is one of the most important factors to relate the three diester-alkaloids content in the decoctions. SN - 1001-4454 UR - https://www.unboundmedicine.com/medline/citation/22500426/[Determination_of_content_changes_of_three_diester_diterpenoid_alkaloids_in_compatibility_of_radix_aconiti_laterlis_preparata_and_Rhizoma_pinelliae_Fructus_trichosanthis_Bulbus_fritillariae_Radix_ampelopsis_Rhizoma_bletillae_by_HPLC]_ DB - PRIME DP - Unbound Medicine ER -