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[HPLC fingerprint analysis of acetoacetate extraction of Polygonum orientale].
Zhong Yao Cai. 2011 Nov; 34(11):1690-4.ZY

Abstract

OBJECTIVE

To establish the HPLC fingerprint analysis method for the quality control of acetoacetate extraction of Polygonum orientale.

METHODS

Agilent C18 (4.6 mm x 250 mm, 5 microm); DAD detector; Mobile phase: methyl alcohol-water gradient elution at a flow rate of 1.0 mL/min, and at a column temperature of 30 degrees C.

RESULTS

26 peaks were selected as the common fingerprint peaks. The relative standard deviations for relative retention values were less than 3% in the precision and repeated test.

CONCLUSION

The repetition, stability and precision of the method is good and it can be used to control the quality of Polygonum orientale.

Authors+Show Affiliations

Hu JX
School of Chemistry and Engineering, Wuhan University of Technology, Wuhan 430070, China. hujiaxing2008@163.com
Lou YC
No affiliation info available
Wang C
No affiliation info available
Zhao L
No affiliation info available
Zhang DQ
No affiliation info available

MeSH

AcetoacetatesAntineoplastic AgentsChromatography, High Pressure LiquidDrugs, Chinese HerbalPlants, MedicinalPolygonumQuality ControlReproducibility of Results

Pub Type(s)

English Abstract
Journal Article
Research Support, Non-U.S. Gov't

Language

chi

PubMed ID

22506389

Citation

Hu, Jia-Xing, et al. "[HPLC Fingerprint Analysis of Acetoacetate Extraction of Polygonum Orientale]." Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, vol. 34, no. 11, 2011, pp. 1690-4.
Hu JX, Lou YC, Wang C, et al. [HPLC fingerprint analysis of acetoacetate extraction of Polygonum orientale]. Zhong Yao Cai. 2011;34(11):1690-4.
Hu, J. X., Lou, Y. C., Wang, C., Zhao, L., & Zhang, D. Q. (2011). [HPLC fingerprint analysis of acetoacetate extraction of Polygonum orientale]. Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, 34(11), 1690-4.
Hu JX, et al. [HPLC Fingerprint Analysis of Acetoacetate Extraction of Polygonum Orientale]. Zhong Yao Cai. 2011;34(11):1690-4. PubMed PMID: 22506389.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [HPLC fingerprint analysis of acetoacetate extraction of Polygonum orientale]. AU - Hu,Jia-Xing, AU - Lou,Yi-Ceng, AU - Wang,Chen, AU - Zhao,Ling, AU - Zhang,Du-Qian, PY - 2012/4/18/entrez PY - 2012/4/18/pubmed PY - 2012/9/25/medline SP - 1690 EP - 4 JF - Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials JO - Zhong Yao Cai VL - 34 IS - 11 N2 - OBJECTIVE: To establish the HPLC fingerprint analysis method for the quality control of acetoacetate extraction of Polygonum orientale. METHODS: Agilent C18 (4.6 mm x 250 mm, 5 microm); DAD detector; Mobile phase: methyl alcohol-water gradient elution at a flow rate of 1.0 mL/min, and at a column temperature of 30 degrees C. RESULTS: 26 peaks were selected as the common fingerprint peaks. The relative standard deviations for relative retention values were less than 3% in the precision and repeated test. CONCLUSION: The repetition, stability and precision of the method is good and it can be used to control the quality of Polygonum orientale. SN - 1001-4454 UR - https://www.unboundmedicine.com/medline/citation/22506389/[HPLC_fingerprint_analysis_of_acetoacetate_extraction_of_Polygonum_orientale]_ DB - PRIME DP - Unbound Medicine ER -