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Validation of a method for the analysis of biogenic amines: histamine instability during wine sample storage.
Anal Chim Acta. 2012 Jun 30; 732:114-9.AC

Abstract

This paper reports on the development of an optimized method for the simultaneous analysis of eight biogenic amines (histamine, methylamine, ethylamine, tyramine, putrescine, cadaverine, phenethylamine, and isoamylamine). The analytical method thus proposed has the following advantages: the easy derivatization of wine, the quantification of biogenic amines and a complete degradation of excess derivatization reagent during sample preparation in order to preserve the column. It consists in reversed phase separation by HPLC and UV-vis detection of the aminoenones formed by the reaction of amino compounds with the derivatization reagent diethyl ethoxymethylenemalonate (DEEMM). The usefulness of this technique was confirmed by an alternative oenological analytical method for the validation, quality control and uncertainty assessment (OIV Oeno 10/2005). The method was validated and proposed as a reference method to the International Organization of Vine and Wine (OIV). As a specific application of the proposed method, the biogenic amine content of Rhône valley wines was investigated.

Authors+Show Affiliations

School of Engineering at Changins, University of Applied Sciences Western Switzerland, Nyon, Switzerland. benoit.bach@eichangins.chNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't
Validation Study

Language

eng

PubMed ID

22688042

Citation

Bach, Benoit, et al. "Validation of a Method for the Analysis of Biogenic Amines: Histamine Instability During Wine Sample Storage." Analytica Chimica Acta, vol. 732, 2012, pp. 114-9.
Bach B, Le Quere S, Vuchot P, et al. Validation of a method for the analysis of biogenic amines: histamine instability during wine sample storage. Anal Chim Acta. 2012;732:114-9.
Bach, B., Le Quere, S., Vuchot, P., Grinbaum, M., & Barnavon, L. (2012). Validation of a method for the analysis of biogenic amines: histamine instability during wine sample storage. Analytica Chimica Acta, 732, 114-9. https://doi.org/10.1016/j.aca.2011.12.036
Bach B, et al. Validation of a Method for the Analysis of Biogenic Amines: Histamine Instability During Wine Sample Storage. Anal Chim Acta. 2012 Jun 30;732:114-9. PubMed PMID: 22688042.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Validation of a method for the analysis of biogenic amines: histamine instability during wine sample storage. AU - Bach,Benoit, AU - Le Quere,Stephanie, AU - Vuchot,Patrick, AU - Grinbaum,Magali, AU - Barnavon,Laurent, Y1 - 2011/12/27/ PY - 2011/08/06/received PY - 2011/12/09/revised PY - 2011/12/17/accepted PY - 2012/6/13/entrez PY - 2012/6/13/pubmed PY - 2012/10/2/medline SP - 114 EP - 9 JF - Analytica chimica acta JO - Anal. Chim. Acta VL - 732 N2 - This paper reports on the development of an optimized method for the simultaneous analysis of eight biogenic amines (histamine, methylamine, ethylamine, tyramine, putrescine, cadaverine, phenethylamine, and isoamylamine). The analytical method thus proposed has the following advantages: the easy derivatization of wine, the quantification of biogenic amines and a complete degradation of excess derivatization reagent during sample preparation in order to preserve the column. It consists in reversed phase separation by HPLC and UV-vis detection of the aminoenones formed by the reaction of amino compounds with the derivatization reagent diethyl ethoxymethylenemalonate (DEEMM). The usefulness of this technique was confirmed by an alternative oenological analytical method for the validation, quality control and uncertainty assessment (OIV Oeno 10/2005). The method was validated and proposed as a reference method to the International Organization of Vine and Wine (OIV). As a specific application of the proposed method, the biogenic amine content of Rhône valley wines was investigated. SN - 1873-4324 UR - https://www.unboundmedicine.com/medline/citation/22688042/Validation_of_a_method_for_the_analysis_of_biogenic_amines:_histamine_instability_during_wine_sample_storage_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0003-2670(11)01736-3 DB - PRIME DP - Unbound Medicine ER -