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Anthocyanin identification and composition of wild Vitis spp. accessions by using LC-MS and LC-NMR.
Anal Chim Acta. 2012 Jun 30; 732:145-52.AC

Abstract

The composition and concentration of anthocyanins of grape berry skins were analyzed in order to assess phenotypic variation between four grape wine varieties belonging to 4 different species: Vitis vinifera, Vitis amurensis, Vitis cinerea and Vitis X champinii. High-performance liquid chromatography coupled to mass spectrometry (LC-MS) and NMR spectroscopy (LC-NMR) were used to separate and identify the structure of anthocyanins present in these species. Combination of LC-MS and LC-NMR data resulted in the identification of 33 anthocyanins. In particular, newly reported cis isomers of p-coumaric-derivatives were identified (petunidin-, peonidin- and malvidin-3-(6-p-coumaroyl)-5-diglucoside). In V. cinerea and V. vinifera, anthocyanins were monoglucoside derivatives whereas in V. amurensis and V. X champinii, both mono- and diglucoside derivatives were identified. Malvidin-, delphinidin- and petunidin-derivatives were, respectively, the most abundant components in V. cinerea and V. vinifera, V. amurensis and V. X champinii.

Authors+Show Affiliations

Université de Bordeaux, ISVV, EA 3675 GESVAB, 33882 Villenave d'Ornon, France.No affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

22688046

Citation

Acevedo De la Cruz, Alexander, et al. "Anthocyanin Identification and Composition of Wild Vitis Spp. Accessions By Using LC-MS and LC-NMR." Analytica Chimica Acta, vol. 732, 2012, pp. 145-52.
Acevedo De la Cruz A, Hilbert G, Rivière C, et al. Anthocyanin identification and composition of wild Vitis spp. accessions by using LC-MS and LC-NMR. Anal Chim Acta. 2012;732:145-52.
Acevedo De la Cruz, A., Hilbert, G., Rivière, C., Mengin, V., Ollat, N., Bordenave, L., Decroocq, S., Delaunay, J. C., Delrot, S., Mérillon, J. M., Monti, J. P., Gomès, E., & Richard, T. (2012). Anthocyanin identification and composition of wild Vitis spp. accessions by using LC-MS and LC-NMR. Analytica Chimica Acta, 732, 145-52. https://doi.org/10.1016/j.aca.2011.11.060
Acevedo De la Cruz A, et al. Anthocyanin Identification and Composition of Wild Vitis Spp. Accessions By Using LC-MS and LC-NMR. Anal Chim Acta. 2012 Jun 30;732:145-52. PubMed PMID: 22688046.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Anthocyanin identification and composition of wild Vitis spp. accessions by using LC-MS and LC-NMR. AU - Acevedo De la Cruz,Alexander, AU - Hilbert,Ghislaine, AU - Rivière,Céline, AU - Mengin,Virginie, AU - Ollat,Nathalie, AU - Bordenave,Louis, AU - Decroocq,Stéphane, AU - Delaunay,Jean-Claude, AU - Delrot,Serge, AU - Mérillon,Jean-Michel, AU - Monti,Jean-Pierre, AU - Gomès,Eric, AU - Richard,Tristan, Y1 - 2011/12/07/ PY - 2011/09/01/received PY - 2011/11/23/revised PY - 2011/11/25/accepted PY - 2012/6/13/entrez PY - 2012/6/13/pubmed PY - 2012/10/2/medline SP - 145 EP - 52 JF - Analytica chimica acta JO - Anal Chim Acta VL - 732 N2 - The composition and concentration of anthocyanins of grape berry skins were analyzed in order to assess phenotypic variation between four grape wine varieties belonging to 4 different species: Vitis vinifera, Vitis amurensis, Vitis cinerea and Vitis X champinii. High-performance liquid chromatography coupled to mass spectrometry (LC-MS) and NMR spectroscopy (LC-NMR) were used to separate and identify the structure of anthocyanins present in these species. Combination of LC-MS and LC-NMR data resulted in the identification of 33 anthocyanins. In particular, newly reported cis isomers of p-coumaric-derivatives were identified (petunidin-, peonidin- and malvidin-3-(6-p-coumaroyl)-5-diglucoside). In V. cinerea and V. vinifera, anthocyanins were monoglucoside derivatives whereas in V. amurensis and V. X champinii, both mono- and diglucoside derivatives were identified. Malvidin-, delphinidin- and petunidin-derivatives were, respectively, the most abundant components in V. cinerea and V. vinifera, V. amurensis and V. X champinii. SN - 1873-4324 UR - https://www.unboundmedicine.com/medline/citation/22688046/Anthocyanin_identification_and_composition_of_wild_Vitis_spp__accessions_by_using_LC_MS_and_LC_NMR_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0003-2670(11)01628-X DB - PRIME DP - Unbound Medicine ER -