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Microwave distillation followed by headspace single drop microextraction coupled to gas chromatography-mass spectrometry (GC-MS) for fast analysis of volatile components of Echinophora platyloba DC.
Food Chem. 2013 May 01; 138(1):251-5.FC

Abstract

To avoid the traditional and time consuming hydrodistillation, the analyses of volatile components in aerial parts of Echinophora platyloba DC was carried out by a simple microwave distillation followed by headspace single drop microextraction (MD-HS-SDME) coupled to gas chromatography-mass spectrometry (GC-MS). The headspace volatile compounds were collected after irradiation using a single drop of n-heptadecan. The extraction conditions were optimised using the relative peak areas as index. The chemical composition of the MD-HS-SDME extracts was confirmed according to their retention indexes and mass spectra. Fifty-three components were extracted and identified by using the MD-HS-SDME method. E-β-ocimene (53.81%), R-D-decalactone (12.75%), α-pinene (6.43%), n-heptanol (6.27%), β-phellanderne (2.70%) and linalool (1.89%) were the major constituents.

Authors+Show Affiliations

Department of Analytical Chemistry, Faculty of Chemistry, Razi University, Kermanshah, Iran. mbgholivand@yahoo.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Evaluation Study
Journal Article

Language

eng

PubMed ID

23265484

Citation

Gholivand, Mohammad Bagher, et al. "Microwave Distillation Followed By Headspace Single Drop Microextraction Coupled to Gas Chromatography-mass Spectrometry (GC-MS) for Fast Analysis of Volatile Components of Echinophora Platyloba DC." Food Chemistry, vol. 138, no. 1, 2013, pp. 251-5.
Gholivand MB, Abolghasemi MM, Piryaei M, et al. Microwave distillation followed by headspace single drop microextraction coupled to gas chromatography-mass spectrometry (GC-MS) for fast analysis of volatile components of Echinophora platyloba DC. Food Chem. 2013;138(1):251-5.
Gholivand, M. B., Abolghasemi, M. M., Piryaei, M., Maassoumi, S. M., & Papzan, A. (2013). Microwave distillation followed by headspace single drop microextraction coupled to gas chromatography-mass spectrometry (GC-MS) for fast analysis of volatile components of Echinophora platyloba DC. Food Chemistry, 138(1), 251-5. https://doi.org/10.1016/j.foodchem.2012.09.112
Gholivand MB, et al. Microwave Distillation Followed By Headspace Single Drop Microextraction Coupled to Gas Chromatography-mass Spectrometry (GC-MS) for Fast Analysis of Volatile Components of Echinophora Platyloba DC. Food Chem. 2013 May 1;138(1):251-5. PubMed PMID: 23265484.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Microwave distillation followed by headspace single drop microextraction coupled to gas chromatography-mass spectrometry (GC-MS) for fast analysis of volatile components of Echinophora platyloba DC. AU - Gholivand,Mohammad Bagher, AU - Abolghasemi,Mir Mahdi, AU - Piryaei,Marzieh, AU - Maassoumi,Sayed Mohammad, AU - Papzan,Abdolhamid, Y1 - 2012/11/08/ PY - 2011/05/10/received PY - 2011/10/31/revised PY - 2012/09/30/accepted PY - 2012/12/26/entrez PY - 2012/12/26/pubmed PY - 2013/6/19/medline SP - 251 EP - 5 JF - Food chemistry JO - Food Chem VL - 138 IS - 1 N2 - To avoid the traditional and time consuming hydrodistillation, the analyses of volatile components in aerial parts of Echinophora platyloba DC was carried out by a simple microwave distillation followed by headspace single drop microextraction (MD-HS-SDME) coupled to gas chromatography-mass spectrometry (GC-MS). The headspace volatile compounds were collected after irradiation using a single drop of n-heptadecan. The extraction conditions were optimised using the relative peak areas as index. The chemical composition of the MD-HS-SDME extracts was confirmed according to their retention indexes and mass spectra. Fifty-three components were extracted and identified by using the MD-HS-SDME method. E-β-ocimene (53.81%), R-D-decalactone (12.75%), α-pinene (6.43%), n-heptanol (6.27%), β-phellanderne (2.70%) and linalool (1.89%) were the major constituents. SN - 1873-7072 UR - https://www.unboundmedicine.com/medline/citation/23265484/Microwave_distillation_followed_by_headspace_single_drop_microextraction_coupled_to_gas_chromatography_mass_spectrometry__GC_MS__for_fast_analysis_of_volatile_components_of_Echinophora_platyloba_DC_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0308-8146(12)01571-3 DB - PRIME DP - Unbound Medicine ER -