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[HPLC fingerprint of compound xueshuantong capsule].
Zhong Yao Cai. 2012 Nov; 35(11):1854-8.ZY

Abstract

OBJECTIVE

To establish the HPLC fingerprint of Compound Xueshuantong Capsule.

METHODS

Dionex Acclaim 120 C18 column (4.6 mm x 150 mm, 3 microm) was used with acetonitrile (A) and 0.05% phosphoric acid (B) in gradient elution mode. The elution profile was:0-50 min (15%-->34% A), 50-95 min (34%-->75% A); The detective wavelength was 203 nm and 270 nm. The column temperature was set at 25 degrees C and the flow rate was 1.0 mL/min.

RESULTS

In the established fingerprint,42 common peaks covering 4 medicinal materials were detected, and 23 chemical compounds were identified by RRLC/MS/MS and DAD spetra.

CONCLUSION

The method can be used for quality control of Compound Xueshuantong Capsule with great precision, accuracy and good reproducibility.

Authors+Show Affiliations

Liang JP
School of Life Sciences, Sun Yat-sen University, Guangzhou 510275, China. liangjp2@163.com
Liu ZZ
No affiliation info available
Peng W
No affiliation info available
Su WW
No affiliation info available

MeSH

AbietanesCapsulesChromatography, High Pressure LiquidDrugs, Chinese HerbalPanax notoginsengPlants, MedicinalQuality ControlReproducibility of ResultsSalvia miltiorrhizaSaponins

Pub Type(s)

Journal Article

Language

chi

PubMed ID

23627102

Citation

Liang, Jie-Ping, et al. "[HPLC Fingerprint of Compound Xueshuantong Capsule]." Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, vol. 35, no. 11, 2012, pp. 1854-8.
Liang JP, Liu ZZ, Peng W, et al. [HPLC fingerprint of compound xueshuantong capsule]. Zhong Yao Cai. 2012;35(11):1854-8.
Liang, J. P., Liu, Z. Z., Peng, W., & Su, W. W. (2012). [HPLC fingerprint of compound xueshuantong capsule]. Zhong Yao Cai = Zhongyaocai = Journal of Chinese Medicinal Materials, 35(11), 1854-8.
Liang JP, et al. [HPLC Fingerprint of Compound Xueshuantong Capsule]. Zhong Yao Cai. 2012;35(11):1854-8. PubMed PMID: 23627102.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [HPLC fingerprint of compound xueshuantong capsule]. AU - Liang,Jie-Ping, AU - Liu,Zhong-Zheng, AU - Peng,Wei, AU - Su,Wei-Wei, PY - 2013/5/1/entrez PY - 2013/5/1/pubmed PY - 2013/11/15/medline SP - 1854 EP - 8 JF - Zhong yao cai = Zhongyaocai = Journal of Chinese medicinal materials JO - Zhong Yao Cai VL - 35 IS - 11 N2 - OBJECTIVE: To establish the HPLC fingerprint of Compound Xueshuantong Capsule. METHODS: Dionex Acclaim 120 C18 column (4.6 mm x 150 mm, 3 microm) was used with acetonitrile (A) and 0.05% phosphoric acid (B) in gradient elution mode. The elution profile was:0-50 min (15%-->34% A), 50-95 min (34%-->75% A); The detective wavelength was 203 nm and 270 nm. The column temperature was set at 25 degrees C and the flow rate was 1.0 mL/min. RESULTS: In the established fingerprint,42 common peaks covering 4 medicinal materials were detected, and 23 chemical compounds were identified by RRLC/MS/MS and DAD spetra. CONCLUSION: The method can be used for quality control of Compound Xueshuantong Capsule with great precision, accuracy and good reproducibility. SN - 1001-4454 UR - https://www.unboundmedicine.com/medline/citation/23627102/[HPLC_fingerprint_of_compound_xueshuantong_capsule]_ DB - PRIME DP - Unbound Medicine ER -