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Development of sample preparation method for eleutheroside B and E analysis in Acanthopanax senticosus by ionic liquids-ultrasound based extraction and high-performance liquid chromatography detection.
Food Chem. 2013 Dec 01; 141(3):2426-33.FC

Abstract

An ionic liquids-based ultrasonic-assisted extraction (ILUAE) method was successfully developed for extracting eleutheroside B and E from Radix Acanthopanax senticosus. Thirteen 1-alkyl-3-methylimidazolium ionic liquids with different cations and anions were investigated and 1-butyl-3-methylimidazolium bromide ([C4mim]Br) solution was selected as the solvent. The conditions for ILUAE, including the ionic liquid concentration, soaking time, ultrasonic power, ultrasonic time, solid-liquid ratio and number of extraction cycles, were optimized. With the proposed method, the energy consumption time was reduced to 30 min, whereas conventional method requires about 4h. The proposed method had good recovery (97.96-103.39%) and reproducibility (RSD, n=5; 3.3% for eleutheroside B, 4.6% for eleutheroside E). ILUAE was an efficient, rapid and simple sample preparation technique that showed high reproducibility and was environmental friendly.

Authors+Show Affiliations

Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, 150040 Harbin, China. ylnefu@163.comNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info availableNo affiliation info available

Pub Type(s)

Evaluation Study
Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

23870977

Citation

Yang, Lei, et al. "Development of Sample Preparation Method for Eleutheroside B and E Analysis in Acanthopanax Senticosus By Ionic Liquids-ultrasound Based Extraction and High-performance Liquid Chromatography Detection." Food Chemistry, vol. 141, no. 3, 2013, pp. 2426-33.
Yang L, Ge H, Wang W, et al. Development of sample preparation method for eleutheroside B and E analysis in Acanthopanax senticosus by ionic liquids-ultrasound based extraction and high-performance liquid chromatography detection. Food Chem. 2013;141(3):2426-33.
Yang, L., Ge, H., Wang, W., Zu, Y., Yang, F., Zhao, C., Zhang, L., & Zhang, Y. (2013). Development of sample preparation method for eleutheroside B and E analysis in Acanthopanax senticosus by ionic liquids-ultrasound based extraction and high-performance liquid chromatography detection. Food Chemistry, 141(3), 2426-33. https://doi.org/10.1016/j.foodchem.2013.05.094
Yang L, et al. Development of Sample Preparation Method for Eleutheroside B and E Analysis in Acanthopanax Senticosus By Ionic Liquids-ultrasound Based Extraction and High-performance Liquid Chromatography Detection. Food Chem. 2013 Dec 1;141(3):2426-33. PubMed PMID: 23870977.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Development of sample preparation method for eleutheroside B and E analysis in Acanthopanax senticosus by ionic liquids-ultrasound based extraction and high-performance liquid chromatography detection. AU - Yang,Lei, AU - Ge,Hongshuang, AU - Wang,Wenjie, AU - Zu,Yuangang, AU - Yang,Fengjian, AU - Zhao,Chunjian, AU - Zhang,Lin, AU - Zhang,Ying, Y1 - 2013/05/25/ PY - 2011/08/11/received PY - 2013/01/18/revised PY - 2013/05/16/accepted PY - 2013/7/23/entrez PY - 2013/7/23/pubmed PY - 2014/2/1/medline KW - Acanthopanax senticosus KW - Eleutheroside B KW - Eleutheroside E KW - Ionic liquid KW - Response surface methodology KW - Ultrasonic-assisted extraction SP - 2426 EP - 33 JF - Food chemistry JO - Food Chem VL - 141 IS - 3 N2 - An ionic liquids-based ultrasonic-assisted extraction (ILUAE) method was successfully developed for extracting eleutheroside B and E from Radix Acanthopanax senticosus. Thirteen 1-alkyl-3-methylimidazolium ionic liquids with different cations and anions were investigated and 1-butyl-3-methylimidazolium bromide ([C4mim]Br) solution was selected as the solvent. The conditions for ILUAE, including the ionic liquid concentration, soaking time, ultrasonic power, ultrasonic time, solid-liquid ratio and number of extraction cycles, were optimized. With the proposed method, the energy consumption time was reduced to 30 min, whereas conventional method requires about 4h. The proposed method had good recovery (97.96-103.39%) and reproducibility (RSD, n=5; 3.3% for eleutheroside B, 4.6% for eleutheroside E). ILUAE was an efficient, rapid and simple sample preparation technique that showed high reproducibility and was environmental friendly. SN - 1873-7072 UR - https://www.unboundmedicine.com/medline/citation/23870977/Development_of_sample_preparation_method_for_eleutheroside_B_and_E_analysis_in_Acanthopanax_senticosus_by_ionic_liquids_ultrasound_based_extraction_and_high_performance_liquid_chromatography_detection_ DB - PRIME DP - Unbound Medicine ER -