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Simultaneous determination of selected biogenic amines in alcoholic beverage samples by isotachophoretic and chromatographic methods.

Abstract

A simple and useful method for the determination of biogenic amines in beverage samples based on isotachophoretic separation is described. The proposed procedure permitted simultaneous analysis of histamine, tyramine, cadaverine, putrescine, tryptamine, 2-phenylethylamine, spermine and spermidine. The data presented demonstrate the utility, simplicity, flexibility, sensitivity and environmentally friendly character of the proposed method. The precision of the method expressed as coefficient of variations varied from 0.1% to 5.9% for beverage samples, whereas recoveries varied from 91% to 101%. The results for the determination of biogenic amines were compared with an HPLC procedure based on a pre-column derivatisation reaction of biogenic amines with dansyl chloride. Furthermore, the derivatisation procedure was optimised by verification of concentration and pH of the buffer, the addition of organic solvents, reaction time and temperature.

Authors+Show Affiliations

a Faculty of Chemistry , Nicolaus Copernicus University , Toruń , Poland.No affiliation info availableNo affiliation info available

Pub Type(s)

Comparative Study
Evaluation Study
Journal Article
Research Support, Non-U.S. Gov't

Language

eng

PubMed ID

24350674

Citation

Jastrzębska, Aneta, et al. "Simultaneous Determination of Selected Biogenic Amines in Alcoholic Beverage Samples By Isotachophoretic and Chromatographic Methods." Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment, vol. 31, no. 1, 2014, pp. 83-92.
Jastrzębska A, Piasta A, Szłyk E. Simultaneous determination of selected biogenic amines in alcoholic beverage samples by isotachophoretic and chromatographic methods. Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2014;31(1):83-92.
Jastrzębska, A., Piasta, A., & Szłyk, E. (2014). Simultaneous determination of selected biogenic amines in alcoholic beverage samples by isotachophoretic and chromatographic methods. Food Additives & Contaminants. Part A, Chemistry, Analysis, Control, Exposure & Risk Assessment, 31(1), 83-92. https://doi.org/10.1080/19440049.2013.855326
Jastrzębska A, Piasta A, Szłyk E. Simultaneous Determination of Selected Biogenic Amines in Alcoholic Beverage Samples By Isotachophoretic and Chromatographic Methods. Food Addit Contam Part A Chem Anal Control Expo Risk Assess. 2014;31(1):83-92. PubMed PMID: 24350674.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Simultaneous determination of selected biogenic amines in alcoholic beverage samples by isotachophoretic and chromatographic methods. AU - Jastrzębska,Aneta, AU - Piasta,Anna, AU - Szłyk,Edward, Y1 - 2013/12/19/ PY - 2013/12/20/entrez PY - 2013/12/20/pubmed PY - 2014/9/27/medline SP - 83 EP - 92 JF - Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment JO - Food Addit Contam Part A Chem Anal Control Expo Risk Assess VL - 31 IS - 1 N2 - A simple and useful method for the determination of biogenic amines in beverage samples based on isotachophoretic separation is described. The proposed procedure permitted simultaneous analysis of histamine, tyramine, cadaverine, putrescine, tryptamine, 2-phenylethylamine, spermine and spermidine. The data presented demonstrate the utility, simplicity, flexibility, sensitivity and environmentally friendly character of the proposed method. The precision of the method expressed as coefficient of variations varied from 0.1% to 5.9% for beverage samples, whereas recoveries varied from 91% to 101%. The results for the determination of biogenic amines were compared with an HPLC procedure based on a pre-column derivatisation reaction of biogenic amines with dansyl chloride. Furthermore, the derivatisation procedure was optimised by verification of concentration and pH of the buffer, the addition of organic solvents, reaction time and temperature. SN - 1944-0057 UR - https://www.unboundmedicine.com/medline/citation/24350674/Simultaneous_determination_of_selected_biogenic_amines_in_alcoholic_beverage_samples_by_isotachophoretic_and_chromatographic_methods_ L2 - http://www.tandfonline.com/doi/full/10.1080/19440049.2013.855326 DB - PRIME DP - Unbound Medicine ER -