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Quality assurance of histamine analysis in fresh and canned fish.
Food Chem. 2016 Nov 15; 211:100-6.FC

Abstract

Histamine determination is relevant for fish safety, quality and trade. Recently a study by the European Union (EU) compared the Codex and the EU mandated methods for the analysis of histamine and observed that they underestimated and overestimated the results, respectively. To solve this problem, a simple and efficient procedure for the extraction and quantification of histamine by ion-pair HPLC method with post-column derivatization and fluorimetric detection is proposed. It was optimized and validated for the analysis of histamine in fish. The method attended the performance criteria established by Commission Decision 2002/657/CE. The method was also submitted to proficiency testing; uncertainty was calculated; and the stability of solutions and standards was investigated. There was no matrix effect. The LOD, LOQ, CCα and CCβ were fit for the purpose. The method was successfully used in the analyses of freshwater fish and fresh and canned tuna.

Authors+Show Affiliations

LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil; Laboratório de Controle de Qualidade de Produtos Farmaceuticos e Cosmeticos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil.LBqA - Laboratório de Bioquímica de Alimentos, Faculdade de Farmácia, Universidade Federal de Minas Gerais, Av. Pres. Antônio Carlos 6627, 31270-901 Belo Horizonte, MG, Brazil. Electronic address: mbeatriz@ufmg.br.

Pub Type(s)

Journal Article

Language

eng

PubMed ID

27283612

Citation

Evangelista, Warlley P., et al. "Quality Assurance of Histamine Analysis in Fresh and Canned Fish." Food Chemistry, vol. 211, 2016, pp. 100-6.
Evangelista WP, Silva TM, Guidi LR, et al. Quality assurance of histamine analysis in fresh and canned fish. Food Chem. 2016;211:100-6.
Evangelista, W. P., Silva, T. M., Guidi, L. R., Tette, P. A., Byrro, R. M., Santiago-Silva, P., Fernandes, C., & Gloria, M. B. (2016). Quality assurance of histamine analysis in fresh and canned fish. Food Chemistry, 211, 100-6. https://doi.org/10.1016/j.foodchem.2016.05.035
Evangelista WP, et al. Quality Assurance of Histamine Analysis in Fresh and Canned Fish. Food Chem. 2016 Nov 15;211:100-6. PubMed PMID: 27283612.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Quality assurance of histamine analysis in fresh and canned fish. AU - Evangelista,Warlley P, AU - Silva,Tarliane M, AU - Guidi,Letícia R, AU - Tette,Patrícia A S, AU - Byrro,Ricardo M D, AU - Santiago-Silva,Paula, AU - Fernandes,Christian, AU - Gloria,Maria Beatriz A, Y1 - 2016/05/06/ PY - 2015/10/05/received PY - 2016/02/02/revised PY - 2016/05/03/accepted PY - 2016/6/11/entrez PY - 2016/6/11/pubmed PY - 2017/1/12/medline KW - Agmatine (PubChem CID: 2794990) KW - Cadaverine (PubChem CID: 80282) KW - Fish KW - Histamine (PubChem CID: 5818) KW - Histamine analysis KW - Matrix effect KW - Phenylethylamine (PubChem CID: 9075) KW - Proficiency test KW - Putrescine (PubChem CID: 9532) KW - Serotonin (PubChem CID: 160436) KW - Spermidine (PubChem CID: 9539) KW - Spermine (PubChem CID: 9384) KW - Tryptamine (PubChem CID: 67652) KW - Tyramine (PubChem CID: 66449) KW - Uncertainty SP - 100 EP - 6 JF - Food chemistry JO - Food Chem VL - 211 N2 - Histamine determination is relevant for fish safety, quality and trade. Recently a study by the European Union (EU) compared the Codex and the EU mandated methods for the analysis of histamine and observed that they underestimated and overestimated the results, respectively. To solve this problem, a simple and efficient procedure for the extraction and quantification of histamine by ion-pair HPLC method with post-column derivatization and fluorimetric detection is proposed. It was optimized and validated for the analysis of histamine in fish. The method attended the performance criteria established by Commission Decision 2002/657/CE. The method was also submitted to proficiency testing; uncertainty was calculated; and the stability of solutions and standards was investigated. There was no matrix effect. The LOD, LOQ, CCα and CCβ were fit for the purpose. The method was successfully used in the analyses of freshwater fish and fresh and canned tuna. SN - 1873-7072 UR - https://www.unboundmedicine.com/medline/citation/27283612/Quality_assurance_of_histamine_analysis_in_fresh_and_canned_fish_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0308-8146(16)30715-4 DB - PRIME DP - Unbound Medicine ER -