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Preparation of multifunctional chitin nanowhiskers/ZnO-Ag NPs and their effect on the properties of carboxymethyl cellulose-based nanocomposite film.
Carbohydr Polym. 2017 Aug 01; 169:467-479.CP

Abstract

Chitin nanowhiskers (ChNW) were isolated and used for the synthesis of hybrid ChNW/ZnO-Ag NPs. The hybrid nanoparticles were used for the preparation of multifunctional carboxymethyl cellulose (CMC) films. A ChNW was needle shape with the width of 8-40nm, the length of 150-260nm, and crystallinity index of 93.6%. The ZnO-Ag NPs were spherical with the diameter of 10.5-16.2nm. STEM, EDX, XRD, and UV-vis analyses confirmed the formation of ZnO-Ag NPs on the surface of ChNW. The thermal stability of ChNW was increased by incorporation of ZnO-Ag NPs. A CMC-based nanocomposite film incorporated with 5wt% of ChNW/ZnO-Ag NPs was homogeneous and showed the high UV-barrier property. The tensile strength (TS) and elastic modulus (E) of the composite film increased by 18-32% and 55-100%, respectively, while the elongation at break (EB) decreased by 23-33%. CMC composite films showed strong antibacterial activity against E. coli and L. monocytogenes.

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Authors+Show Affiliations

Oun AA
Department of Food Engineering and Bionanocomposite Research Institute, Mokpo National University, 61 Dorimri, Chungkyemyon, Muangun, Jeonnam, 534-729, Republic of Korea; Food Engineering and Packaging Department, Food Technology Research Institute, Agricultural Research Center, Giza, Egypt.
Rhim JW
Center for Humanities and Sciences, and Department of Food and Nutrition, Kyung Hee University, 26 Kyungheedae-ro, Dongdaemun-gu, Seoul 120-701, Republic of Korea. Electronic address: jwrhim@mokpo.ac.kr.

MeSH

Anti-Bacterial AgentsCarboxymethylcellulose SodiumChitinEscherichia coliListeria monocytogenesMetal NanoparticlesNanocompositesSilverZinc Oxide

Pub Type(s)

Journal Article

Language

eng

PubMed ID

28504170

Citation

Oun, Ahmed A., and Jong-Whan Rhim. "Preparation of Multifunctional Chitin nanowhiskers/ZnO-Ag NPs and Their Effect On the Properties of Carboxymethyl Cellulose-based Nanocomposite Film." Carbohydrate Polymers, vol. 169, 2017, pp. 467-479.
Oun AA, Rhim JW. Preparation of multifunctional chitin nanowhiskers/ZnO-Ag NPs and their effect on the properties of carboxymethyl cellulose-based nanocomposite film. Carbohydr Polym. 2017;169:467-479.
Oun, A. A., & Rhim, J. W. (2017). Preparation of multifunctional chitin nanowhiskers/ZnO-Ag NPs and their effect on the properties of carboxymethyl cellulose-based nanocomposite film. Carbohydrate Polymers, 169, 467-479. https://doi.org/10.1016/j.carbpol.2017.04.042
Oun AA, Rhim JW. Preparation of Multifunctional Chitin nanowhiskers/ZnO-Ag NPs and Their Effect On the Properties of Carboxymethyl Cellulose-based Nanocomposite Film. Carbohydr Polym. 2017 Aug 1;169:467-479. PubMed PMID: 28504170.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Preparation of multifunctional chitin nanowhiskers/ZnO-Ag NPs and their effect on the properties of carboxymethyl cellulose-based nanocomposite film. AU - Oun,Ahmed A, AU - Rhim,Jong-Whan, Y1 - 2017/04/22/ PY - 2017/01/16/received PY - 2017/04/14/revised PY - 2017/04/18/accepted PY - 2017/5/16/entrez PY - 2017/5/16/pubmed PY - 2018/7/19/medline KW - Antimicrobial activity KW - Carboxymethyl cellulose KW - Chitin nanowhiskers KW - Hybrid nanoparticles KW - Multifunctional nanocomposite KW - ZnO-Ag nanoparticles SP - 467 EP - 479 JF - Carbohydrate polymers JO - Carbohydr Polym VL - 169 N2 - Chitin nanowhiskers (ChNW) were isolated and used for the synthesis of hybrid ChNW/ZnO-Ag NPs. The hybrid nanoparticles were used for the preparation of multifunctional carboxymethyl cellulose (CMC) films. A ChNW was needle shape with the width of 8-40nm, the length of 150-260nm, and crystallinity index of 93.6%. The ZnO-Ag NPs were spherical with the diameter of 10.5-16.2nm. STEM, EDX, XRD, and UV-vis analyses confirmed the formation of ZnO-Ag NPs on the surface of ChNW. The thermal stability of ChNW was increased by incorporation of ZnO-Ag NPs. A CMC-based nanocomposite film incorporated with 5wt% of ChNW/ZnO-Ag NPs was homogeneous and showed the high UV-barrier property. The tensile strength (TS) and elastic modulus (E) of the composite film increased by 18-32% and 55-100%, respectively, while the elongation at break (EB) decreased by 23-33%. CMC composite films showed strong antibacterial activity against E. coli and L. monocytogenes. SN - 1879-1344 UR - https://www.unboundmedicine.com/medline/citation/28504170/Preparation_of_multifunctional_chitin_nanowhiskers/ZnO_Ag_NPs_and_their_effect_on_the_properties_of_carboxymethyl_cellulose_based_nanocomposite_film_ L2 - https://linkinghub.elsevier.com/retrieve/pii/S0144-8617(17)30431-9 DB - PRIME DP - Unbound Medicine ER -