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[Preparation and quality standard of standard decoction of Phellodendri Chinensis Cortex pieces].
Zhongguo Zhong Yao Za Zhi. 2018 Mar; 43(5):873-878.ZZ

Abstract

To prepare standard decoction of Phellodendri Chinensis Cortex pieces, establish quality standards, and provide reference for evaluating the quality of formula granule of Phellodendri Chinensis Cortex. 15 batches Phellodendri Chinensis Cortex pieces in different levels of quality were collected from market. The standard extraction process was used to prepare the standard decoction, and then the transfer rate of the index components berberine and phellodendrine was calculated to measure dry extraction ratio and pH value. So the method for Phellodendri Chinensis Cortex's fingerprint and content determination of index components was established. The result revealed that the extraction ratio was from 12.81% to 19.41%, with an average value of 16.54%. The transfer rate of berberine was at the range of 36.4%-56.6%, with an average value of 48.9%. The transfer rate of Phellodendri Chinensis Cortex piece was at the range of 47.5%-83.3%, with an average value of 63.1%. The pH value was between 5.2 and 5.9. The Similarity Evaluation System for Chromatographic Fingerprint of traditional Chinese medicine TCM (2012A) was used to analyze and compare the fingerprint and the similarity between the fingerprint of formula granule of Phellodendri Chinensis Cortex and the reference fingerprint was over 0.9. The preparation method in this paper showed good precision, stability and repeatability in fingerprint analysis, suitable for quality evaluation of Phellodendri Chinensis Cortex pieces standard decoction.

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Authors+Show Affiliations

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China. Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

MeSH

BerberineDrugs, Chinese HerbalPhellodendronQuality ControlQuinolizines

Pub Type(s)

Journal Article

Language

chi

PubMed ID

29676081

Citation

Wang, Shu-Hui, et al. "[Preparation and Quality Standard of Standard Decoction of Phellodendri Chinensis Cortex Pieces]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 43, no. 5, 2018, pp. 873-878.

Wang SH, Deng Z, Zhang J, et al. [Preparation and quality standard of standard decoction of Phellodendri Chinensis Cortex pieces]. Zhongguo Zhong Yao Za Zhi. 2018;43(5):873-878.

Wang, S. H., Deng, Z., Zhang, J., Jiao, M. J., Zhang, G. Y., Shi, J., Cheng, J. T., & Liu, A. (2018). [Preparation and quality standard of standard decoction of Phellodendri Chinensis Cortex pieces]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 43(5), 873-878. https://doi.org/10.19540/j.cnki.cjcmm.20180105.012

Wang SH, et al. [Preparation and Quality Standard of Standard Decoction of Phellodendri Chinensis Cortex Pieces]. Zhongguo Zhong Yao Za Zhi. 2018;43(5):873-878. PubMed PMID: 29676081.

* Article titles in AMA citation format should be in sentence-case

TY - JOUR T1 - [Preparation and quality standard of standard decoction of Phellodendri Chinensis Cortex pieces]. AU - Wang,Shu-Hui, AU - Deng,Zhe, AU - Zhang,Jun, AU - Jiao,Meng-Jiao, AU - Zhang,Guo-Yuan, AU - Shi,Jia, AU - Cheng,Jin-Tang, AU - Liu,An, PY - 2017/10/12/received PY - 2018/4/21/entrez PY - 2018/4/21/pubmed PY - 2019/7/13/medline KW - Phellodendri Chinensis Cortex pieces KW - quality standard KW - standard decoction SP - 873 EP - 878 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 43 IS - 5 N2 - To prepare standard decoction of Phellodendri Chinensis Cortex pieces, establish quality standards, and provide reference for evaluating the quality of formula granule of Phellodendri Chinensis Cortex. 15 batches Phellodendri Chinensis Cortex pieces in different levels of quality were collected from market. The standard extraction process was used to prepare the standard decoction, and then the transfer rate of the index components berberine and phellodendrine was calculated to measure dry extraction ratio and pH value. So the method for Phellodendri Chinensis Cortex's fingerprint and content determination of index components was established. The result revealed that the extraction ratio was from 12.81% to 19.41%, with an average value of 16.54%. The transfer rate of berberine was at the range of 36.4%-56.6%, with an average value of 48.9%. The transfer rate of Phellodendri Chinensis Cortex piece was at the range of 47.5%-83.3%, with an average value of 63.1%. The pH value was between 5.2 and 5.9. The Similarity Evaluation System for Chromatographic Fingerprint of traditional Chinese medicine TCM (2012A) was used to analyze and compare the fingerprint and the similarity between the fingerprint of formula granule of Phellodendri Chinensis Cortex and the reference fingerprint was over 0.9. The preparation method in this paper showed good precision, stability and repeatability in fingerprint analysis, suitable for quality evaluation of Phellodendri Chinensis Cortex pieces standard decoction. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/29676081/[Preparation_and_quality_standard_of_standard_decoction_of_Phellodendri_Chinensis_Cortex_pieces]_ DB - PRIME DP - Unbound Medicine ER -