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[Research on standard decoction of processed Curcumae Longae Rhizoma containing volatile oil].
Zhongguo Zhong Yao Za Zhi. 2018 Mar; 43(5):879-884.ZZ

Abstract

To prepare processed Curcumae Longae Rhizoma standard decoction, establish its quality standard, provides quality reference for formulated Jianghuang granules and lay a foundation for standard decoction research for the pieces containing volatile oil. Thirteen batches of processed Curcumae Longae Rhizoma standard decoctions were prepared according to the preparation requirements for standard decoction of Chinese herbal medicine containing volatile oil. With curcumin as the detection index, the transfer rate and extraction ratio were calculated; the pH value was determined and HPLC fingerprint analysis method was established. The results showed that the transfer rate ranged from 0.67% to 2.24%; the extraction rate was at a range of 9.95% to 18.36% and pH value was 3.86 to 6.05. Then the Similarity Evaluation System for Chromatographic Fingerprint of Traditional Chinese Medicine (2012A) was used to analyze and compare the fingerprint. Sixteen common peaks were determined and three were identified including bisdemethoxycurcumin (peak 7), demethoxycurcumin (peak 8) and curcumin (peak 9). Moreover, the similarity was over 0.78 in the similarity evaluation of 13 batches of samples. HPLC fingerprint analysis method of processed Curcumae Longae Rhizoma standard decoction was established, showing good precision, stability and repeatability with certain identification effect, suitable for the quality control of formulated Jianghuang granules.

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Publisher Full Text (DOI)

Authors+Show Affiliations

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China. Jiangxi University of Traditional Chinese Medicine, Nanchang 330004, China.

Shanghai University of Traditional Chinese Medicine, Shanghai 201203, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

Key Laboratory of Beijing for Identification and Safety Evaluation of Chinese Medicine， Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences, Beijing 100700, China.

MeSH

Chromatography, High Pressure LiquidCurcumaDrugs, Chinese HerbalMedicine, Chinese TraditionalOils, VolatileQuality ControlRhizome

Pub Type(s)

Journal Article

Language

chi

PubMed ID

29676082

Citation

Deng, Zhe, et al. "[Research On Standard Decoction of Processed Curcumae Longae Rhizoma Containing Volatile Oil]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 43, no. 5, 2018, pp. 879-884.

Deng Z, Zhang F, Jiao MJ, et al. [Research on standard decoction of processed Curcumae Longae Rhizoma containing volatile oil]. Zhongguo Zhong Yao Za Zhi. 2018;43(5):879-884.

Deng, Z., Zhang, F., Jiao, M. J., Zhang, J., Shi, J., Cheng, J. T., & Liu, A. (2018). [Research on standard decoction of processed Curcumae Longae Rhizoma containing volatile oil]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 43(5), 879-884. https://doi.org/10.19540/j.cnki.cjcmm.20180105.013

Deng Z, et al. [Research On Standard Decoction of Processed Curcumae Longae Rhizoma Containing Volatile Oil]. Zhongguo Zhong Yao Za Zhi. 2018;43(5):879-884. PubMed PMID: 29676082.

* Article titles in AMA citation format should be in sentence-case

TY - JOUR T1 - [Research on standard decoction of processed Curcumae Longae Rhizoma containing volatile oil]. AU - Deng,Zhe, AU - Zhang,Fan, AU - Jiao,Meng-Jiao, AU - Zhang,Jun, AU - Shi,Jia, AU - Cheng,Jin-Tang, AU - Liu,An, PY - 2017/10/12/received PY - 2018/4/21/entrez PY - 2018/4/21/pubmed PY - 2019/7/13/medline KW - fingerprint KW - processed Curcumae Longae Rhizoma KW - standard decoction KW - volatile oil SP - 879 EP - 884 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 43 IS - 5 N2 - To prepare processed Curcumae Longae Rhizoma standard decoction, establish its quality standard, provides quality reference for formulated Jianghuang granules and lay a foundation for standard decoction research for the pieces containing volatile oil. Thirteen batches of processed Curcumae Longae Rhizoma standard decoctions were prepared according to the preparation requirements for standard decoction of Chinese herbal medicine containing volatile oil. With curcumin as the detection index, the transfer rate and extraction ratio were calculated; the pH value was determined and HPLC fingerprint analysis method was established. The results showed that the transfer rate ranged from 0.67% to 2.24%; the extraction rate was at a range of 9.95% to 18.36% and pH value was 3.86 to 6.05. Then the Similarity Evaluation System for Chromatographic Fingerprint of Traditional Chinese Medicine (2012A) was used to analyze and compare the fingerprint. Sixteen common peaks were determined and three were identified including bisdemethoxycurcumin (peak 7), demethoxycurcumin (peak 8) and curcumin (peak 9). Moreover, the similarity was over 0.78 in the similarity evaluation of 13 batches of samples. HPLC fingerprint analysis method of processed Curcumae Longae Rhizoma standard decoction was established, showing good precision, stability and repeatability with certain identification effect, suitable for the quality control of formulated Jianghuang granules. SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/29676082/[Research_on_standard_decoction_of_processed_Curcumae_Longae_Rhizoma_containing_volatile_oil]_ DB - PRIME DP - Unbound Medicine ER -