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[Single-Laboratory Validation Study of Determination of Patulin by GC-MS in Juice].
Shokuhin Eiseigaku Zasshi. 2018; 59(3):157-160.SE

Abstract

We examined whether the analytical method of patulin (a mycotoxin found in fruit juice) developed in Nagano prefecture meets the criteria in the Codex Procedural Manual and Guidelines on Analytical Terminology. The trueness, repeatability, within-laboratory reproducibility and HorRat value were 98.8-103.4%, less than 6.4, 8.1 and 0.4%, respectively, for apple juice and pear juice.Thus, the trueness and precision met the required criteria.

Authors+Show Affiliations

Food and Agricultural Materials Inspection Center, Kobe Regional Center.Food and Agricultural Materials Inspection Center, Kobe Regional Center.Food and Agricultural Materials Inspection Center, Headquarters Saitama Shintoshin National Government Building Kensato BLDG.Food and Agricultural Materials Inspection Center, Headquarters Saitama Shintoshin National Government Building Kensato BLDG.

Pub Type(s)

Journal Article

Language

jpn

PubMed ID

30033994

Citation

Hattori, Satoshi, et al. "[Single-Laboratory Validation Study of Determination of Patulin By GC-MS in Juice]." Shokuhin Eiseigaku Zasshi. Journal of the Food Hygienic Society of Japan, vol. 59, no. 3, 2018, pp. 157-160.
Hattori S, Tsukada M, Morita M, et al. [Single-Laboratory Validation Study of Determination of Patulin by GC-MS in Juice]. Shokuhin Eiseigaku Zasshi. 2018;59(3):157-160.
Hattori, S., Tsukada, M., Morita, M., & Suenaga, K. (2018). [Single-Laboratory Validation Study of Determination of Patulin by GC-MS in Juice]. Shokuhin Eiseigaku Zasshi. Journal of the Food Hygienic Society of Japan, 59(3), 157-160. https://doi.org/10.3358/shokueishi.59.157
Hattori S, et al. [Single-Laboratory Validation Study of Determination of Patulin By GC-MS in Juice]. Shokuhin Eiseigaku Zasshi. 2018;59(3):157-160. PubMed PMID: 30033994.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Single-Laboratory Validation Study of Determination of Patulin by GC-MS in Juice]. AU - Hattori,Satoshi, AU - Tsukada,Masanori, AU - Morita,Mifumi, AU - Suenaga,Kazuya, PY - 2018/7/24/entrez PY - 2018/7/24/pubmed PY - 2019/6/22/medline KW - GC-MS KW - apple juice KW - patulin KW - pear juice KW - validation study SP - 157 EP - 160 JF - Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan JO - Shokuhin Eiseigaku Zasshi VL - 59 IS - 3 N2 - We examined whether the analytical method of patulin (a mycotoxin found in fruit juice) developed in Nagano prefecture meets the criteria in the Codex Procedural Manual and Guidelines on Analytical Terminology. The trueness, repeatability, within-laboratory reproducibility and HorRat value were 98.8-103.4%, less than 6.4, 8.1 and 0.4%, respectively, for apple juice and pear juice.Thus, the trueness and precision met the required criteria. SN - 0015-6426 UR - https://www.unboundmedicine.com/medline/citation/30033994/[Single_Laboratory_Validation_Study_of_Determination_of_Patulin_by_GC_MS_in_Juice]_ L2 - https://dx.doi.org/10.3358/shokueishi.59.157 DB - PRIME DP - Unbound Medicine ER -