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Characterization of the polyphenolic fraction of pomegranate samples by comprehensive two-dimensional liquid chromatography coupled to mass spectrometry detection.
Nat Prod Res. 2020 Jan; 34(1):39-45.NP

Abstract

Punica granatum L., commonly known as pomegranate, is an ancient fruit widely consumed all over the world as fresh fruit or juice. In addition, it is extensively used in therapeutic formulas, cosmetics and food seasonings. The fruit is native to Afghanistan, Iran, China and the Indian sub-continent. The pomegranate market has steadily grown, presumably due to the increasing demand of health-conscious consumers for products with potential beneficial effects on human health, due to the synergistic presence of a unique and complex phytochemical composition that enclose anthocyanins, phenolic acids and hydrolysable tannins. Conventionally, for their analysis liquid chromatography is employed even though it can present some drawbacks in terms of resolving power. In this contribution, as a valuable alternative, comprehensive two-dimensional liquid chromatography with "shifted gradients" in the second dimension, was applied for the characterization of three pomegranate samples, leading to the identification of 37 different polyphenolic compounds.

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Publisher Full Text (DOI)

Authors+Show Affiliations

Russo M
Unit of Food Science and Nutrition, Department of Medicine, University Campus Bio-Medico of Rome, Rome, Italy.
Cacciola F
Dipartimento di Scienze Biomediche, Odontoiatriche e delle Immagini Morfologiche e Funzionali, University of Messina, Messina, Italy.
Arena K
Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali, University of Messina, Messina, Italy.
Mangraviti D
Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali, University of Messina, Messina, Italy.
de Gara L
Unit of Food Science and Nutrition, Department of Medicine, University Campus Bio-Medico of Rome, Rome, Italy.
Dugo P
Unit of Food Science and Nutrition, Department of Medicine, University Campus Bio-Medico of Rome, Rome, Italy. Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali, University of Messina, Messina, Italy. Chromaleont s.r.l., c/o Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali, University of Messina, Messina, Italy.
Mondello L
Unit of Food Science and Nutrition, Department of Medicine, University Campus Bio-Medico of Rome, Rome, Italy. Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali, University of Messina, Messina, Italy. Chromaleont s.r.l., c/o Dipartimento di Scienze Chimiche, Biologiche, Farmaceutiche ed Ambientali, University of Messina, Messina, Italy.

MeSH

AnthocyaninsChromatography, LiquidFruitHumansHydrolyzable TanninsLythraceaeMass SpectrometryPhytochemicalsPlant ExtractsPolyphenolsPomegranate

Pub Type(s)

Journal Article

Language

eng

PubMed ID

30691301

Citation

Russo, Marina, et al. "Characterization of the Polyphenolic Fraction of Pomegranate Samples By Comprehensive Two-dimensional Liquid Chromatography Coupled to Mass Spectrometry Detection." Natural Product Research, vol. 34, no. 1, 2020, pp. 39-45.
Russo M, Cacciola F, Arena K, et al. Characterization of the polyphenolic fraction of pomegranate samples by comprehensive two-dimensional liquid chromatography coupled to mass spectrometry detection. Nat Prod Res. 2020;34(1):39-45.
Russo, M., Cacciola, F., Arena, K., Mangraviti, D., de Gara, L., Dugo, P., & Mondello, L. (2020). Characterization of the polyphenolic fraction of pomegranate samples by comprehensive two-dimensional liquid chromatography coupled to mass spectrometry detection. Natural Product Research, 34(1), 39-45. https://doi.org/10.1080/14786419.2018.1561690
Russo M, et al. Characterization of the Polyphenolic Fraction of Pomegranate Samples By Comprehensive Two-dimensional Liquid Chromatography Coupled to Mass Spectrometry Detection. Nat Prod Res. 2020;34(1):39-45. PubMed PMID: 30691301.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Characterization of the polyphenolic fraction of pomegranate samples by comprehensive two-dimensional liquid chromatography coupled to mass spectrometry detection. AU - Russo,Marina, AU - Cacciola,Francesco, AU - Arena,Katia, AU - Mangraviti,Domenica, AU - de Gara,Laura, AU - Dugo,Paola, AU - Mondello,Luigi, Y1 - 2019/01/29/ PY - 2019/1/30/pubmed PY - 2020/3/11/medline PY - 2019/1/30/entrez KW - Punica granatum L. KW - comprehensive two-dimensional liquid chromatography KW - mass spectrometry KW - polyphenols SP - 39 EP - 45 JF - Natural product research JO - Nat Prod Res VL - 34 IS - 1 N2 - Punica granatum L., commonly known as pomegranate, is an ancient fruit widely consumed all over the world as fresh fruit or juice. In addition, it is extensively used in therapeutic formulas, cosmetics and food seasonings. The fruit is native to Afghanistan, Iran, China and the Indian sub-continent. The pomegranate market has steadily grown, presumably due to the increasing demand of health-conscious consumers for products with potential beneficial effects on human health, due to the synergistic presence of a unique and complex phytochemical composition that enclose anthocyanins, phenolic acids and hydrolysable tannins. Conventionally, for their analysis liquid chromatography is employed even though it can present some drawbacks in terms of resolving power. In this contribution, as a valuable alternative, comprehensive two-dimensional liquid chromatography with "shifted gradients" in the second dimension, was applied for the characterization of three pomegranate samples, leading to the identification of 37 different polyphenolic compounds. SN - 1478-6427 UR - https://www.unboundmedicine.com/medline/citation/30691301/Characterization_of_the_polyphenolic_fraction_of_pomegranate_samples_by_comprehensive_two_dimensional_liquid_chromatography_coupled_to_mass_spectrometry_detection_ DB - PRIME DP - Unbound Medicine ER -