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Inter-Varietal Diversity of Typical Volatile and Phenolic Profiles of Croatian Extra Virgin Olive Oils as Revealed by GC-IT-MS and UPLC-DAD Analysis.
Foods. 2019 Nov 09; 8(11)F

Abstract

Despite having an interesting native olive gene pool and a rapidly emerging olive oil industry, monovarietal extra virgin olive oils (EVOO) from Croatia are relatively unexplored. To investigate the inter-varietal diversity of typical volatile and phenolic profiles of Croatian EVOO, 93 samples from six olive (Olea europaea L.) varieties were subjected to gas chromatography-ion trap mass spectrometry (GC-IT-MS) and ultra-performance liquid chromatography with diode array detection (UPLC-DAD), respectively. Quantitative descriptive sensory analysis was also performed. Analysis of variance extracted many relevant exclusive or partial discriminators between monovarietal EVOOs among the identified volatile compounds and phenols. Successful differentiation model with a 100% correct classification was built by linear discriminant analysis, while the most typical volatiles for each monovarietal EVOO were confirmed by partial least squares discriminant analysis. Diverse typical sensory attributes among the EVOOs were tentatively ascribed to the variations in the composition of volatiles and phenols. It was proven that the approach that comprises GC-IT-MS and UPLC-DAD analysis may provide additional objective information about varietal origin and typicity which successfully complement those obtained by sensory analysis. The approach was characterized as universal in nature, with a significant potential to contribute in strengthening the varietal identities and position on the market of monovarietal and Protected Denomination of Origin (PDO) EVOO.

Authors+Show Affiliations

Institute of Agriculture and Tourism, Karla Huguesa 8, HR-52440 Poreč, Croatia. Centre of Excellence for Biodiversity and Molecular Plant Breeding, Svetošimunska 25, HR-10000 Zagreb, Croatia.Institute of Agriculture and Tourism, Karla Huguesa 8, HR-52440 Poreč, Croatia.Institute for Adriatic Crops and Karst Reclamation, Put Duilova 11, HR-21000 Split, Croatia.Institute of Agriculture and Tourism, Karla Huguesa 8, HR-52440 Poreč, Croatia.Institute of Agriculture and Tourism, Karla Huguesa 8, HR-52440 Poreč, Croatia.Institute of Agriculture and Tourism, Karla Huguesa 8, HR-52440 Poreč, Croatia.

Pub Type(s)

Journal Article

Language

eng

PubMed ID

31717549

Citation

Lukić, Igor, et al. "Inter-Varietal Diversity of Typical Volatile and Phenolic Profiles of Croatian Extra Virgin Olive Oils as Revealed By GC-IT-MS and UPLC-DAD Analysis." Foods (Basel, Switzerland), vol. 8, no. 11, 2019.
Lukić I, Lukić M, Žanetić M, et al. Inter-Varietal Diversity of Typical Volatile and Phenolic Profiles of Croatian Extra Virgin Olive Oils as Revealed by GC-IT-MS and UPLC-DAD Analysis. Foods. 2019;8(11).
Lukić, I., Lukić, M., Žanetić, M., Krapac, M., Godena, S., & Brkić Bubola, K. (2019). Inter-Varietal Diversity of Typical Volatile and Phenolic Profiles of Croatian Extra Virgin Olive Oils as Revealed by GC-IT-MS and UPLC-DAD Analysis. Foods (Basel, Switzerland), 8(11). https://doi.org/10.3390/foods8110565
Lukić I, et al. Inter-Varietal Diversity of Typical Volatile and Phenolic Profiles of Croatian Extra Virgin Olive Oils as Revealed By GC-IT-MS and UPLC-DAD Analysis. Foods. 2019 Nov 9;8(11) PubMed PMID: 31717549.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Inter-Varietal Diversity of Typical Volatile and Phenolic Profiles of Croatian Extra Virgin Olive Oils as Revealed by GC-IT-MS and UPLC-DAD Analysis. AU - Lukić,Igor, AU - Lukić,Marina, AU - Žanetić,Mirella, AU - Krapac,Marin, AU - Godena,Sara, AU - Brkić Bubola,Karolina, Y1 - 2019/11/09/ PY - 2019/10/11/received PY - 2019/11/03/revised PY - 2019/11/06/accepted PY - 2019/11/14/entrez PY - 2019/11/14/pubmed PY - 2019/11/14/medline KW - extra virgin olive oil KW - phenols KW - sensory quality KW - varietal typicity KW - volatile compounds JF - Foods (Basel, Switzerland) JO - Foods VL - 8 IS - 11 N2 - Despite having an interesting native olive gene pool and a rapidly emerging olive oil industry, monovarietal extra virgin olive oils (EVOO) from Croatia are relatively unexplored. To investigate the inter-varietal diversity of typical volatile and phenolic profiles of Croatian EVOO, 93 samples from six olive (Olea europaea L.) varieties were subjected to gas chromatography-ion trap mass spectrometry (GC-IT-MS) and ultra-performance liquid chromatography with diode array detection (UPLC-DAD), respectively. Quantitative descriptive sensory analysis was also performed. Analysis of variance extracted many relevant exclusive or partial discriminators between monovarietal EVOOs among the identified volatile compounds and phenols. Successful differentiation model with a 100% correct classification was built by linear discriminant analysis, while the most typical volatiles for each monovarietal EVOO were confirmed by partial least squares discriminant analysis. Diverse typical sensory attributes among the EVOOs were tentatively ascribed to the variations in the composition of volatiles and phenols. It was proven that the approach that comprises GC-IT-MS and UPLC-DAD analysis may provide additional objective information about varietal origin and typicity which successfully complement those obtained by sensory analysis. The approach was characterized as universal in nature, with a significant potential to contribute in strengthening the varietal identities and position on the market of monovarietal and Protected Denomination of Origin (PDO) EVOO. SN - 2304-8158 UR - https://www.unboundmedicine.com/medline/citation/31717549/Inter_Varietal_Diversity_of_Typical_Volatile_and_Phenolic_Profiles_of_Croatian_Extra_Virgin_Olive_Oils_as_Revealed_by_GC_IT_MS_and_UPLC_DAD_Analysis_ DB - PRIME DP - Unbound Medicine ER -
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