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Pt-Pd-doped NiO nanoparticle decorated at single-wall carbon nanotubes: An excellent, powerful electrocatalyst for the fabrication of An electrochemical sensor to determine nalbuphine in the presence of tramadol as two opioid analgesic drugs.
J Pharm Biomed Anal. 2020 May 30; 189:113397.JP

Abstract

In this study, a Pt-Pd-doped NiO nanoparticle decorated at the surface of single-wall carbon nanotubes (Pt-Pd/NiO-NPs/SWCNTs) was synthesized using a simple chemical precipitation method and characterized by XRD, TEM, and EDS methods. The results confirmed that Pt-Pd/NiO-NPs/SWCNTs were synthesized with good purity and at the nanoscale size. Moreover, a highly sensitive electroanalytical sensor was fabricated by incorporating synthesized Pt-Pd/NiO-NPs/SWCNT nanocomposites into a carbon paste electrode (CPE) in the presence of 1-ethyl-3-methylimidazolium methanesulfonate (EMICH3SO3-) as binder. The Pt-Pd/NiO-NPs/SWCNTs/EMICH3SO3-/CPE showed a powerful electro-catalytic activity for electro-oxidation of nalbuphine, and the results confirmed that the oxidation of nalbuphine was improved 6.34 times and relative oxidation potential was decreased about 110 mV compared to unmodified electrodes. The Pt-Pd/NiO-NPs/SWCNTs/EMICH3SO3-/CPE also showed good catalytic activity for the determination of nalbuphine in the presence of tramadol and the oxidation potential of these opioid analgesic drugs separated with ΔE =460 mV. In the final step, the Pt-Pd/NiO-NPs/SWCNTs/EMICH3SO3-/CPE was used to determine nalbuphine with a detection limit of 0.9 nM and tramadol with a detection limit of 50.0 nM in drug samples. The results confirmed the powerful and interesting ability of the sensor in the analysis of a real sample.

Authors+Show Affiliations

Department of Chemistry, University of Sistan and Baluchestan, Iran.Department of Chemistry, University of Sistan and Baluchestan, Iran. Electronic address: ali@hamoon.usb.ac.ir.Nanostructure Based Biosensors Research Group, Ton Duc Thang University, Ho Chi Minh City, Vietnam; Faculty of Applied Sciences, Ton Duc Thang University, Ho Chi Minh City, Vietnam. Electronic address: hassan.karimi.maleh@tdtu.edu.vn.

Pub Type(s)

Journal Article

Language

eng

PubMed ID

32563934

Citation

Tavana, Toktam, et al. "Pt-Pd-doped NiO Nanoparticle Decorated at Single-wall Carbon Nanotubes: an Excellent, Powerful Electrocatalyst for the Fabrication of an Electrochemical Sensor to Determine Nalbuphine in the Presence of Tramadol as Two Opioid Analgesic Drugs." Journal of Pharmaceutical and Biomedical Analysis, vol. 189, 2020, p. 113397.
Tavana T, Rezvani AR, Karimi-Maleh H. Pt-Pd-doped NiO nanoparticle decorated at single-wall carbon nanotubes: An excellent, powerful electrocatalyst for the fabrication of An electrochemical sensor to determine nalbuphine in the presence of tramadol as two opioid analgesic drugs. J Pharm Biomed Anal. 2020;189:113397.
Tavana, T., Rezvani, A. R., & Karimi-Maleh, H. (2020). Pt-Pd-doped NiO nanoparticle decorated at single-wall carbon nanotubes: An excellent, powerful electrocatalyst for the fabrication of An electrochemical sensor to determine nalbuphine in the presence of tramadol as two opioid analgesic drugs. Journal of Pharmaceutical and Biomedical Analysis, 189, 113397. https://doi.org/10.1016/j.jpba.2020.113397
Tavana T, Rezvani AR, Karimi-Maleh H. Pt-Pd-doped NiO Nanoparticle Decorated at Single-wall Carbon Nanotubes: an Excellent, Powerful Electrocatalyst for the Fabrication of an Electrochemical Sensor to Determine Nalbuphine in the Presence of Tramadol as Two Opioid Analgesic Drugs. J Pharm Biomed Anal. 2020 May 30;189:113397. PubMed PMID: 32563934.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Pt-Pd-doped NiO nanoparticle decorated at single-wall carbon nanotubes: An excellent, powerful electrocatalyst for the fabrication of An electrochemical sensor to determine nalbuphine in the presence of tramadol as two opioid analgesic drugs. AU - Tavana,Toktam, AU - Rezvani,Ali Reza, AU - Karimi-Maleh,Hassan, Y1 - 2020/05/30/ PY - 2020/02/23/received PY - 2020/05/25/revised PY - 2020/05/26/accepted PY - 2020/6/22/pubmed PY - 2020/6/22/medline PY - 2020/6/22/entrez KW - 1-Ethyl-3-methylimidazolium methanesulfonate KW - Nalbuphine KW - Pt-Pd-doped NiO nanoparticle-decorated single-wall carbon nanotubes KW - Tramadol SP - 113397 EP - 113397 JF - Journal of pharmaceutical and biomedical analysis JO - J Pharm Biomed Anal VL - 189 N2 - In this study, a Pt-Pd-doped NiO nanoparticle decorated at the surface of single-wall carbon nanotubes (Pt-Pd/NiO-NPs/SWCNTs) was synthesized using a simple chemical precipitation method and characterized by XRD, TEM, and EDS methods. The results confirmed that Pt-Pd/NiO-NPs/SWCNTs were synthesized with good purity and at the nanoscale size. Moreover, a highly sensitive electroanalytical sensor was fabricated by incorporating synthesized Pt-Pd/NiO-NPs/SWCNT nanocomposites into a carbon paste electrode (CPE) in the presence of 1-ethyl-3-methylimidazolium methanesulfonate (EMICH3SO3-) as binder. The Pt-Pd/NiO-NPs/SWCNTs/EMICH3SO3-/CPE showed a powerful electro-catalytic activity for electro-oxidation of nalbuphine, and the results confirmed that the oxidation of nalbuphine was improved 6.34 times and relative oxidation potential was decreased about 110 mV compared to unmodified electrodes. The Pt-Pd/NiO-NPs/SWCNTs/EMICH3SO3-/CPE also showed good catalytic activity for the determination of nalbuphine in the presence of tramadol and the oxidation potential of these opioid analgesic drugs separated with ΔE =460 mV. In the final step, the Pt-Pd/NiO-NPs/SWCNTs/EMICH3SO3-/CPE was used to determine nalbuphine with a detection limit of 0.9 nM and tramadol with a detection limit of 50.0 nM in drug samples. The results confirmed the powerful and interesting ability of the sensor in the analysis of a real sample. SN - 1873-264X UR - https://www.unboundmedicine.com/medline/citation/32563934/Pt-Pd-doped_NiO_nanoparticle_decorated_at_single-wall_carbon_nanotubes:_An_excellent,_powerful_electrocatalyst_for_the_fabrication_of_An_electrochemical_sensor_to_determine_nalbuphine_in_the_presence_of_tramadol_as_two_opioid_analgesic_drugs L2 - https://linkinghub.elsevier.com/retrieve/pii/S0731-7085(20)31283-8 DB - PRIME DP - Unbound Medicine ER -
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