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[Study on quality standard of fried Vaccariae Semen standard decoction].
Zhongguo Zhong Yao Za Zhi. 2020 Sep; 45(18):4398-4403.ZZ

Abstract

According to the preparation principle of standard decoction of Chinese herbal medicines, fourteen batches of fried Vaccariae Semen decoction were prepared in this study and the quality research was carried out to establish a quality evaluation method for the standard decoction of fried Vaccariae Semen. The contents of vaccarin were determined, and its transfer rate from decoction piece to standard decoction was calculated. The extract rate and pH value were measured, and HPLC fingerprint method was established for analysis. The results of the 14 batches of samples revealed that the transfer rates of vaccarin were between 58.98%-93.94%; the extract rates were between 8.67%-17.83%, and the pH values were between 5.55-6.44. Moreover, 9 common chromatographic peaks were identified in fingerprints analysis. The similarities of the 14 batches of samples were analyzed and compared, and the results showed that the similarities were all higher than 0.96. In this study, the preparation process for fried Vaccariae Semen standard decoction was standard, with high similarities in fingerprint. A convenient and reliable method of comprehensive quality evaluation was established in this study, with a high precision, stability and repeatability, which can provide a reference for the quality control of fried Vaccariae Semen standard decoction, dispensing granule and related Chinese classical formulas(decoction).

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Publisher Full Text (DOI)

Authors+Show Affiliations

Shan W
School of Pharmacy, Shaanxi Institute of Internal Trade & Commerce Xi'an 712046, China Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China.
Bo-Nan L
Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China School of Pharmacy, Liaoning University of Traditional Chinese Medicine Dalian 116600, China.
Xin-Lin L
Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China Anhui University of Chinese Medicine Hefei 230000, China.
Jiao-Yan Y
Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China.
Yong-Xin Z
Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China.
Yao-Hua L
Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China.
Ji S
School of Pharmacy, Liaoning University of Traditional Chinese Medicine Dalian 116600, China.
Jing-Jing Z
Institute of Chinese Materia Medica, China Academy of Chinese Medical Sciences Beijing 100700, China.

MeSH

Chromatography, High Pressure LiquidDrugs, Chinese HerbalQuality ControlSemen

Pub Type(s)

Journal Article

Language

chi

PubMed ID

33164368

Citation

Shan, Wang, et al. "[Study On Quality Standard of Fried Vaccariae Semen Standard Decoction]." Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, vol. 45, no. 18, 2020, pp. 4398-4403.
Shan W, Bo-Nan L, Xin-Lin L, et al. [Study on quality standard of fried Vaccariae Semen standard decoction]. Zhongguo Zhong Yao Za Zhi. 2020;45(18):4398-4403.
Shan, W., Bo-Nan, L., Xin-Lin, L., Jiao-Yan, Y., Yong-Xin, Z., Yao-Hua, L., Ji, S., & Jing-Jing, Z. (2020). [Study on quality standard of fried Vaccariae Semen standard decoction]. Zhongguo Zhong Yao Za Zhi = Zhongguo Zhongyao Zazhi = China Journal of Chinese Materia Medica, 45(18), 4398-4403. https://doi.org/10.19540/j.cnki.cjcmm.20200602.302
Shan W, et al. [Study On Quality Standard of Fried Vaccariae Semen Standard Decoction]. Zhongguo Zhong Yao Za Zhi. 2020;45(18):4398-4403. PubMed PMID: 33164368.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - [Study on quality standard of fried Vaccariae Semen standard decoction]. AU - Shan,Wang, AU - Bo-Nan,Liu, AU - Xin-Lin,Lyu, AU - Jiao-Yan,Yang, AU - Yong-Xin,Zhang, AU - Yao-Hua,Liang, AU - Ji,Shi, AU - Jing-Jing,Zhu, PY - 2020/11/9/entrez PY - 2020/11/10/pubmed PY - 2020/11/11/medline KW - fingerprints KW - fried Vaccariae Semen KW - standard decoction KW - vaccarin SP - 4398 EP - 4403 JF - Zhongguo Zhong yao za zhi = Zhongguo zhongyao zazhi = China journal of Chinese materia medica JO - Zhongguo Zhong Yao Za Zhi VL - 45 IS - 18 N2 - According to the preparation principle of standard decoction of Chinese herbal medicines, fourteen batches of fried Vaccariae Semen decoction were prepared in this study and the quality research was carried out to establish a quality evaluation method for the standard decoction of fried Vaccariae Semen. The contents of vaccarin were determined, and its transfer rate from decoction piece to standard decoction was calculated. The extract rate and pH value were measured, and HPLC fingerprint method was established for analysis. The results of the 14 batches of samples revealed that the transfer rates of vaccarin were between 58.98%-93.94%; the extract rates were between 8.67%-17.83%, and the pH values were between 5.55-6.44. Moreover, 9 common chromatographic peaks were identified in fingerprints analysis. The similarities of the 14 batches of samples were analyzed and compared, and the results showed that the similarities were all higher than 0.96. In this study, the preparation process for fried Vaccariae Semen standard decoction was standard, with high similarities in fingerprint. A convenient and reliable method of comprehensive quality evaluation was established in this study, with a high precision, stability and repeatability, which can provide a reference for the quality control of fried Vaccariae Semen standard decoction, dispensing granule and related Chinese classical formulas(decoction). SN - 1001-5302 UR - https://www.unboundmedicine.com/medline/citation/33164368/[Study_on_quality_standard_of_fried_Vaccariae_Semen_standard_decoction]_ DB - PRIME DP - Unbound Medicine ER -