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Characterization of Aroma Compounds in Cooked Sorghum Using Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry and Gas Chromatography-Olfactometry-Mass Spectrometry.
Molecules. 2021 Aug 07; 26(16)M

Abstract

Sorghum is the major raw material for the production of Chinese Baijiu (Chinese liquor) and has a great effect on the flavor of Baijiu. Volatiles in cooked glutinous and non-glutinous sorghum samples were extracted using solid-phase microextraction (SPME) and analyzed via comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry (GC×GC-TOFMS) and gas chromatography-olfactometry/mass spectrometry (GC-O/MS). A total of 145 volatile compounds and 52 potent odorant compounds were identified from both sorghum types according to the retention index, MS, aroma, and standards. Based on their aroma features, the compounds were grouped into eight general categories, and the intensities of each aroma group were summed. Moreover, most of the compounds detected in the cooked sorghums were also detected in commercial Chinese Baijiu, indicating that the aroma compounds produced during the sorghum cooking process have a direct and significant influence on the final flavor quality of Baijiu.

Authors+Show Affiliations

Key Laboratory of Industrial Biotechnology of Ministry of Education, State Key Laboratory of Food Science & Technology, School of Biotechnology, Jiangnan University, Wuxi 214122, China.Technique Center of Kweichow Moutai Co. Ltd., Guizhou 564500, China.Technique Center of Kweichow Moutai Co. Ltd., Guizhou 564500, China.Technique Center of Kweichow Moutai Co. Ltd., Guizhou 564500, China.Technique Center of Kweichow Moutai Co. Ltd., Guizhou 564500, China.Key Laboratory of Industrial Biotechnology of Ministry of Education, State Key Laboratory of Food Science & Technology, School of Biotechnology, Jiangnan University, Wuxi 214122, China.

Pub Type(s)

Journal Article

Language

eng

PubMed ID

34443387

Citation

Chen, Shuang, et al. "Characterization of Aroma Compounds in Cooked Sorghum Using Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry and Gas Chromatography-Olfactometry-Mass Spectrometry." Molecules (Basel, Switzerland), vol. 26, no. 16, 2021.
Chen S, Wang L, Ni D, et al. Characterization of Aroma Compounds in Cooked Sorghum Using Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry and Gas Chromatography-Olfactometry-Mass Spectrometry. Molecules. 2021;26(16).
Chen, S., Wang, L., Ni, D., Lin, L., Wang, H., & Xu, Y. (2021). Characterization of Aroma Compounds in Cooked Sorghum Using Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry and Gas Chromatography-Olfactometry-Mass Spectrometry. Molecules (Basel, Switzerland), 26(16). https://doi.org/10.3390/molecules26164796
Chen S, et al. Characterization of Aroma Compounds in Cooked Sorghum Using Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry and Gas Chromatography-Olfactometry-Mass Spectrometry. Molecules. 2021 Aug 7;26(16) PubMed PMID: 34443387.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Characterization of Aroma Compounds in Cooked Sorghum Using Comprehensive Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry and Gas Chromatography-Olfactometry-Mass Spectrometry. AU - Chen,Shuang, AU - Wang,Li, AU - Ni,Derang, AU - Lin,Lin, AU - Wang,Heyu, AU - Xu,Yan, Y1 - 2021/08/07/ PY - 2021/06/30/received PY - 2021/07/23/revised PY - 2021/08/05/accepted PY - 2021/8/27/entrez PY - 2021/8/28/pubmed PY - 2021/9/18/medline KW - GC-O/MS KW - GC×GC-TOFMS KW - SPME KW - aroma compounds KW - cooked sorghum JF - Molecules (Basel, Switzerland) JO - Molecules VL - 26 IS - 16 N2 - Sorghum is the major raw material for the production of Chinese Baijiu (Chinese liquor) and has a great effect on the flavor of Baijiu. Volatiles in cooked glutinous and non-glutinous sorghum samples were extracted using solid-phase microextraction (SPME) and analyzed via comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry (GC×GC-TOFMS) and gas chromatography-olfactometry/mass spectrometry (GC-O/MS). A total of 145 volatile compounds and 52 potent odorant compounds were identified from both sorghum types according to the retention index, MS, aroma, and standards. Based on their aroma features, the compounds were grouped into eight general categories, and the intensities of each aroma group were summed. Moreover, most of the compounds detected in the cooked sorghums were also detected in commercial Chinese Baijiu, indicating that the aroma compounds produced during the sorghum cooking process have a direct and significant influence on the final flavor quality of Baijiu. SN - 1420-3049 UR - https://www.unboundmedicine.com/medline/citation/34443387/Characterization_of_Aroma_Compounds_in_Cooked_Sorghum_Using_Comprehensive_Two_Dimensional_Gas_Chromatography_Time_of_Flight_Mass_Spectrometry_and_Gas_Chromatography_Olfactometry_Mass_Spectrometry_ DB - PRIME DP - Unbound Medicine ER -