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Exploring multiple-cumulative trapping solid-phase microextraction coupled to gas chromatography-mass spectrometry for quality and authenticity assessment of olive oil.
Food Chem. 2022 Jul 30; 383:132438.FC

Abstract

This study explores the potential of an innovative multi-cumulative trapping headspace solid-phase microextraction approach coupled with untargeted data analysis to enhance the information provided by aroma profiling of virgin olive oil. Sixty-nine samples of different olive oil commercial categories (extra-virgin, virgin and lampante oil) and different geographical origins were analysed using this novel workflow. The results from each sample were aligned and compared using for the first time a tile-based approach to enable the mining of all of the raw data within the chemometrics platform without any pre-processing methods. The data matrix obtained allowed the extraction of multiple-level information from the volatile profile of the samples. Not only was it possible to classify the samples within the commercial category that they belonged to, but the same data also provided interesting information regarding the geographical origin of the extra-virgin olive oil.

Authors+Show Affiliations

DiBEST, University of Calabria, Via Ponte P. Bucci, Cubo 6b, Arcavacata Di Rende, 87036, Italy; Markes International Ltd, 1000B Central Park, Western Avenue, Bridgend, CF31 3RT, UK; Department of Chemical, Pharmaceutical and Agricultural Sciences, University of Ferrara, Via Luigi Borsari, n. 46, Ferrara 44121, UK.Gembloux Agro-Bio Tech, University of Liège, Passage des Déportés 2, Gembloux 5030, Belgium.SepSolve Analytical, 4 Swan Court, Peterborough PE7 8GX, UK.Gembloux Agro-Bio Tech, University of Liège, Passage des Déportés 2, Gembloux 5030, Belgium. Electronic address: gpurcaro@uliege.be.

Pub Type(s)

Journal Article

Language

eng

PubMed ID

35183954

Citation

Spadafora, Natasha D., et al. "Exploring Multiple-cumulative Trapping Solid-phase Microextraction Coupled to Gas Chromatography-mass Spectrometry for Quality and Authenticity Assessment of Olive Oil." Food Chemistry, vol. 383, 2022, p. 132438.
Spadafora ND, Mascrez S, McGregor L, et al. Exploring multiple-cumulative trapping solid-phase microextraction coupled to gas chromatography-mass spectrometry for quality and authenticity assessment of olive oil. Food Chem. 2022;383:132438.
Spadafora, N. D., Mascrez, S., McGregor, L., & Purcaro, G. (2022). Exploring multiple-cumulative trapping solid-phase microextraction coupled to gas chromatography-mass spectrometry for quality and authenticity assessment of olive oil. Food Chemistry, 383, 132438. https://doi.org/10.1016/j.foodchem.2022.132438
Spadafora ND, et al. Exploring Multiple-cumulative Trapping Solid-phase Microextraction Coupled to Gas Chromatography-mass Spectrometry for Quality and Authenticity Assessment of Olive Oil. Food Chem. 2022 Jul 30;383:132438. PubMed PMID: 35183954.
* Article titles in AMA citation format should be in sentence-case
TY - JOUR T1 - Exploring multiple-cumulative trapping solid-phase microextraction coupled to gas chromatography-mass spectrometry for quality and authenticity assessment of olive oil. AU - Spadafora,Natasha D, AU - Mascrez,Steven, AU - McGregor,Laura, AU - Purcaro,Giorgia, Y1 - 2022/02/12/ PY - 2021/08/31/received PY - 2022/02/01/revised PY - 2022/02/09/accepted PY - 2022/2/21/pubmed PY - 2022/4/13/medline PY - 2022/2/20/entrez KW - Authenticity KW - MC-SPME KW - Multiple-cumulative trapping headspace solid-phase microextraction KW - Olive oil KW - Quality KW - Random forest KW - Sensory evaluation SP - 132438 EP - 132438 JF - Food chemistry JO - Food Chem VL - 383 N2 - This study explores the potential of an innovative multi-cumulative trapping headspace solid-phase microextraction approach coupled with untargeted data analysis to enhance the information provided by aroma profiling of virgin olive oil. Sixty-nine samples of different olive oil commercial categories (extra-virgin, virgin and lampante oil) and different geographical origins were analysed using this novel workflow. The results from each sample were aligned and compared using for the first time a tile-based approach to enable the mining of all of the raw data within the chemometrics platform without any pre-processing methods. The data matrix obtained allowed the extraction of multiple-level information from the volatile profile of the samples. Not only was it possible to classify the samples within the commercial category that they belonged to, but the same data also provided interesting information regarding the geographical origin of the extra-virgin olive oil. SN - 1873-7072 UR - https://www.unboundmedicine.com/medline/citation/35183954/Exploring_multiple_cumulative_trapping_solid_phase_microextraction_coupled_to_gas_chromatography_mass_spectrometry_for_quality_and_authenticity_assessment_of_olive_oil_ DB - PRIME DP - Unbound Medicine ER -